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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental started 8th May 2012, experimental phase ended 10th August 2012
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2012
Report date:
2012

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
The melting point was carried out using a Buchi Melting Point Apparatus B-545
GLP compliance:
yes
Type of method:
other: Buchi melting point apparatus

Test material

Constituent 1
Chemical structure
Reference substance name:
lithium 3-((3,4-dicyanophenyl)sulfonyl)propane-1-sulfonate)
EC Number:
700-777-2
Cas Number:
667889-11-4
Molecular formula:
C11H9N2O5S2Li
IUPAC Name:
lithium 3-((3,4-dicyanophenyl)sulfonyl)propane-1-sulfonate)
Test material form:
solid: particulate/powder
Remarks:
migrated information: powder

Results and discussion

Melting / freezing point
Melting / freezing pt.:
> 300 °C
Atm. press.:
> 100 - < 101 kPa
Decomp. temp.:
> 300 °C

Applicant's summary and conclusion

Conclusions:
Using a preliminary temperature gradient of 26°C to 300°C at 5°C/min the melting point was assessed. No melting point was observed.
Executive summary:

Introduction

The study was undertaken to determine the melting point of the test material. The method used was designed to be compatible with OECD Guideline 102.The melting point was carried out using a Buchi melting point apparatus B-545.

Results and Conclusions

No melting point was observed using a preliminary temperature gradient of 26°C to 300°C. MP is greater than 300°C