Registration Dossier
Registration Dossier
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EC number: 907-489-8 | CAS number: -
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- From 23 June 2017 to 23 October 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- 1995
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Version / remarks:
- 2008
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- differential scanning calorimetry
- Specific details on test material used for the study:
- SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: CY71353002
- Expiration date of the lot/batch: 01/06/2019
- Purity test date: 01/06/2017
- Purity of the test item: 99.8% - Melting / freezing pt.:
- -39.1 °C
- Melting / freezing pt.:
- -38.6 °C
- Key result
- Melting / freezing pt.:
- -38.9 °C
- Remarks on result:
- other: mean value
- Conclusions:
- The melting point of the test item was determined to be -38.9°C +/- 0.5°C.
- Executive summary:
The melting point of the test item was determined using the DSC method according to recognised guidelines and under GLP. No deviation from the guidelines was observed during the test.
Before measurements with the test item, the reliability of the apparatus was checked with a reference item. The result obtained was in accordance with the theoretical value, therefore the apparatus was considered conform for the test item melting point determination.
The melting point was determined to be -38.9°C (average of two assays).
Reference
Two assays were performed and complied with the accuracy criteria (+/- 0.5°C up to 326.9°C). In these two assays, the cooling phase was performed from 25°C to -100°C at 10°C/min and a heating phase from -100°C to 100°C at 10°C/min.
Description of key information
The melting point of the test item was determined in a key study of Klimisch validity one, performed according to recognised guideline and under GLP.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- -38.9 °C
Additional information
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
