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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Type of method:
other: melt microscope / differential scanning calorimetry
Melting / freezing pt.:
>= 139.3 - <= 154.6 °C

In the melt microscope an onset-temperature of 140 °C was observed, at 154 °C a cloudy melt could be observed. No clear point was reached up to 210 °C. The clouding is probably sodium chloride.

For the determination of the melting range, the main DSC test was performed in triplicate. The melting ranges were read from the second and the third heating run of each test as extrapolated onset and extrapolated endset of the allocated melting peak. After the test procedure, the samples were re-weighed in order to check for a significant sample loss indicating a potential interfering non-melting processes. For none of the samples a significant weight loss was recorded (<1%).

As an average a melting range of 139.3 °C to 154.6 °C was measured by DSC which is in a good accordance to the visual observation 140 °C (onset-temperature of change) and 154 °C (cloudy melt).

Conclusions:
A melting range of 139.3°C to 154.6°C was determined by DSC (OECD TG 102 / EU method A.1).
Executive summary:

The melting point of C8 -10 Alkylamidopropyl betaine was determined according to OECD Guideline 102 and EU method A.1 using a melt microscope and differential scanning calorimetry. A melting range of 139.3°C to 154.6°C was measured by DSC which is in a good accordance to the visual observation 140°C (onset-temperature of change) and 154°C (cloudy melt).

Description of key information

melting range: 139.3°C to 154.6°C (OECD TG 102 / EU method A.1; melt microscope / differential scanning calorimetry; RL1)

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
140 °C

Additional information

The melting point of C8 -10 Alkylamidopropyl betaine was determined according to OECD Guideline 102 and EU method A.1 using a melt microscope and differential scanning calorimetry. A melting range of 139.3°C to 154.6°C was measured by DSC which is in a good accordance to the visual observation 140°C (onset-temperature of change) and 154°C (cloudy melt).