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Physical & Chemical properties

Melting point / freezing point

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2010-04-01 to 2010-04-19
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Principles of method if other than guideline:
The pratical test performance was based on the in-house test procedure VTA(S)31X93001.02: "Melting temperature determination (Tm) of solid and liquid substances by means of DSC".
GLP compliance:
no
Type of method:
thermal analysis
Remarks:
Differential Scanning Calorimetry
Melting / freezing pt.:
-67 - 18 °C
Remarks on result:
other: The cooling run shows a crystallisation at 12 °C.

The test item shows an area of melting temperatures (in the 1. and 2. heating run) between -67 °C and 18 °C (melting of crystalline parts (according to the definition in the OECD Guideline 102.

The cooling run shows a crystallisation at 12 °C.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Study period:
2011-12-22
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study without detailed documentation
Guideline:
other: ASTM D97-08
GLP compliance:
no
Type of method:
pour point
Melting / freezing pt.:
19 °C
Atm. press.:
ca. 1 013 hPa

Average of two test results 19 °C each. Assumed to be measured at atmospheric pressure.

Description of key information

-67 to 18 °C (OECD 102, DSC method)

Key value for chemical safety assessment

Additional information

Reported pour point: 19 °C.