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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
20.06.2016-29.08.2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
yes (incl. QA statement)
Type of method:
dynamic method
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: 5-2-A
- Expiration date of the lot/batch: 14. Feb. 2017

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: room temperature in a closed vessel
Key result
Boiling pt.:
ca.
Decomposition:
yes
Decomp. temp.:
ca. 320 °C

 Observation First determination     Second determination    
  Thermomter Cottrell Pump Thermometer Sample  Thermometer Cottrell Pump  Thermometer Sample 
 Lots of small bubbles on the bottom and in the pump approx. 94 °C  approx. 280 °C  approx. 119 °C  approx. 280 °C 

 The colour of the test item was slightly yellowish            

 The test item started to boil with consistently superheating maximum 160.9 °C  approx. 320 °C  maximum 155.3 °C  approx. 320 °C 
 Atmospheric pressure 99354 Pa     99575 Pa    

The Cottrell pump could not produce a mixture of vapour and liquid. The experiments were stopped. After cooling down, the test item appearance was yellowish, which indicated decomposition during the experiment.

Conclusions:
No boiling point of Salacos 13 could be determined. Decomposition of the substance occures at about 320 °C.
Executive summary:

For the determination of the boiling point of Salacos 13 the dynamic method was used.

No boiling point of Salacos 13 could be determined. Decomposition of the substance occures at about 320 °C.

Description of key information

No boiling point of Salacos 13 could be determined. Decomposition of the substance occures at about 320 °C.

Key value for chemical safety assessment

Additional information