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Diss Factsheets

Physical & Chemical properties

Density

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Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
13 September 2016 - 17 January 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method
Key result
Type:
relative density
Density:
ca. 9.216
Temp.:
21 °C
Remarks on result:
other: Mean value of two assays (assay No.1: 9.225, assay No.2: 9.207)

Two independent measurements at 21.2°C (assay No. 1) and 20.7°C (assay No. 2) were done. Runs 1 and 2 of assay No. 2 were not taken into account because they did not comply with the quality criterion.

The two assays resulted in relative densities of 9.225 ± 0.008 and 9.207 ± 0.008, respectively. The mean relative density was thus 9.216 ± 0.012 at 21.0°C.

Reference volume (Va) was 79.250 cm3.

Volume of sample cell holder (Vc) was 27.636 cm3.

Test item sample weight was 12.1920 g and 12.2559 g in assay No. 1 and 2, respectively.

The measurements are described in the tables below.

Assay no. 1

 Data

 P2 (PSIG)

 P3 (PSIG)

 VP (cm³)

 Density (g/cm³)

Relative density

 Mean relative density

 Run No. 1

 17.078

 4.257

 1.3224

 9.2199

 9.2201

 

 

 9.225 ± 0.008

 

 

 Run No. 2

 17.078

 4.257

 1.3224

 9.2199

 9.2201

 Run No. 3

 17.085

 4.259

 1.3203

 9.2346

 9.2348

Assay no. 2

 Data

 P2 (PSIG)

 P3 (PSIG)

 VP (cm³)

 Density (g/cm³)

Relative density

 Mean relative density

 Run No. 3

 17.106

 4.263

 1.3304

 9.2122

 9.2124

 

 

 9.207 ± 0.008

 

 

 Run No. 4

 17.082

 4.257

 1.3306

 9.2111

 9.2113

 Run No. 5

 17.099

 4.261

 1.3325

 9.1976

 9.1979

Conclusions:
The relative density of lutetium oxide was determined according to EU A.3 method and OECD test guideline 109 in compliance with GLP using a gas comparison pycnometer. The relative density of the test item was determined to be 9.216 ± 0.012 at 21.0°C.

Description of key information

In a GLP study (K1, Demangel, 2017) based on the OECD 109 guideline and the EC A.3 method, the relative density of the test item was determined to be 9.216 ± 0.012 at 21.0°C. This value is considered the key value for lutetium trioxide.

Key value for chemical safety assessment

Relative density at 20C:
9.216

Additional information