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EC number: 944-802-7 | CAS number: -
Boiling point
Administrative data
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 008
- Report date:
- 2008
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Version / remarks:
- 27 July 1997
- Deviations:
- not specified
- GLP compliance:
- yes
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- Didodecyl hydrogen citrate
- EC Number:
- 247-146-3
- EC Name:
- Didodecyl hydrogen citrate
- Cas Number:
- 25637-88-1
- Molecular formula:
- C30H56O7
- IUPAC Name:
- didodecyl hydrogen citrate
- Reference substance name:
- Dodecyl dihydrogen 2-hydroxypropane-1,2,3-tricarboxylate
- EC Number:
- 278-950-2
- EC Name:
- Dodecyl dihydrogen 2-hydroxypropane-1,2,3-tricarboxylate
- Cas Number:
- 78568-45-3
- Molecular formula:
- C18H32O7
- IUPAC Name:
- 2-[2-(dodecyloxy)-2-oxoethyl]-2-hydroxysuccinic acid
- Reference substance name:
- Tridodecyl 2-hydroxypropane-1,2,3-tricarboxylate
- EC Number:
- 265-671-6
- EC Name:
- Tridodecyl 2-hydroxypropane-1,2,3-tricarboxylate
- Cas Number:
- 65277-53-4
- Molecular formula:
- C42H80O7
- IUPAC Name:
- tridodecyl citrate
- Reference substance name:
- Citric acid
- EC Number:
- 201-069-1
- EC Name:
- Citric acid
- Cas Number:
- 77-92-9
- Molecular formula:
- C6H8O7
- IUPAC Name:
- citric acid
- Reference substance name:
- Dodecan-1-ol
- EC Number:
- 203-982-0
- EC Name:
- Dodecan-1-ol
- Cas Number:
- 112-53-8
- Molecular formula:
- C12H26O
- IUPAC Name:
- dodecan-1-ol
- Reference substance name:
- unidentified impurities
- IUPAC Name:
- unidentified impurities
- Test material form:
- solid: granular
Constituent 1
Constituent 2
Constituent 3
impurity 1
impurity 2
impurity 3
Results and discussion
Boiling point
- Key result
- Boiling pt.:
- >= 275 °C
- Decomposition:
- yes
- Decomp. temp.:
- >= 275 °C
Any other information on results incl. tables
In the DSC curve a small glass transition peak was observed at approximately 0 °C in the first experiment. An endothermic peak was observed between 25 and 75 °C. Melting of the test substance probably caused this effect.The extrapolated onset temperature of this peak was determined to be 35 °C. An endothermic effect started at 275 °C. This effect was due to reaction and/or decomposition of the test substance. After the experiment , a yellow coloured, molten residue remained in the sample container (original colour: white). The change in temperature and colour indicated that the test substance had reacted or fdecomposed.
The second experiment showed essentially the same results a sduring the first experiment.
Applicant's summary and conclusion
- Conclusions:
- Reaction and/or decomposition of the test substance were observed at ca. 275 °C. Boiling of the substance was not observed below the temperature at which reaction and/or decomposition started. Therefore the substance has no boiling temperature.
- Executive summary:
The boiling point of the substance was determined by DSC according to OECD Guideline 103.
The first experiment was performed with 5.48 mg test substance. The sample was heated from -25 °C to 327 °C with a rate of 20 °C/minute.
An amount of 7.78. mg test substance was used during the second experiment.. The same temperature program as with the firdt experiment was applied.
All experiments were performed under a flow of nitrogen and at atmosperic pressure.
In the DSC curve a small glass transition peak was observed at approximately 0 °C in the first experiment. An endothermic peak was observed between 25 and 75 °C. Melting of the test substance probably caused this effect.The extrapolated onset temperature of this peak was determined to be 35 °C. An endothermic effect started at 275 °C. This effect was due to reaction and/or decomposition of the test substance. After the experiment , a yellow coloured, molten residue remained in the sample container (original colour: white). The change in temperature and colour indicated that the test substance had reacted or fdecomposed.
The second experiment showed essentially the same results a sduring the first experiment.
Reaction and/or decomposition of the test substance were observed at ca. 275 °C. Boiling of the substance was not observed below the temperature at which reaction and/or decomposition started. Therefore the substance has no boiling temperature.
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