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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17 September - 14 November 2001
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
- EEC Directive 92/69 Method A1 (1992)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature
Melting / freezing pt.:
< 50.5 °C
Remarks on result:
other: Test substance partially frozen at -50.5 degree C, but temperature did not remain constant

- Assay 1: No freezing point was determined. The test substance was too viscous and hardened, stirring could not be performed below - 15.8 degree C (at 97.1 kPa)

- Assay 2 (without stirring): No freezing point was determined. The test substance was partially frozen at -50.5 degree C, but temperature did not remain constant.

Conclusions:
No freezing point could be determined for the test substance under the current experimental conditions (freezing point < -50.5 °C ).
Executive summary:

A GLP study was conducted according to OECD Guideline No. 102 and EC Method A1 to determine the freezing point of 2,2-bis(chloromethyl)trimethylene bis(bis(2-chloroethyl)phosphate). This study is classified as valid without restrictions and satisfies the guideline requirements.

In a first assay stirring of the test substance was not possible below -15.8 degrees C. In a second assay (without stirring) the temperature at which the test substance was partially frozen, did not remain constant. Under the experimental conditions of this test no freezing point could be determined.

Description of key information

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-50.5 °C

Additional information