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Physical & Chemical properties

Particle size distribution (Granulometry)

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Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
27th February - 27th June 2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted according to EU Test Guidelines at a GLP accredited laboratory
Qualifier:
no guideline followed
Principles of method if other than guideline:
The particle size distribution was examined using sieve analysis. As less than 10% by weight of the test substance was found to pass a 75 micron sieve, no further testing was required.
GLP compliance:
yes (incl. QA statement)
Type of method:
sieving
Type of distribution:
mass based distribution
Percentile:
D50
Remarks on result:
other: Migrated from fields under 'Mass median diameter' as D50 percentile. No source field for Standard deviation.
No.:
#1
Size:
> 400 µm
Distribution:
77.1 %
No.:
#2
Size:
>= 125 - <= 400 µm
Distribution:
17.7 %
No.:
#3
Size:
>= 75 - <= 125 µm
Distribution:
2.7 %
No.:
#4
Size:
>= 30 - <= 75 µm
Distribution:
2 %
No.:
#5
Size:
>= 10 - <= 30 µm
Distribution:
0.5 %
No.:
#6
Size:
< 10 µm
Distribution:
0 %
Conclusions:
The results indicated that 2.5% w/w of T-1620L was smaller than 75 μm.
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
06 January 2017 - 09 January 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187
GLP compliance:
yes (incl. QA statement)
Type of method:
Laser scattering/diffraction
Type of distribution:
mass based distribution
Specific details on test material used for the study:
- Appearance: Pale yellow powder
- Storage conditions: Room temperature (15 to 25°C)
- Batch number: 101X5
- Purity: > 98%
- Expiry date: October 2017
- Date received: 14 November 2016
Mass median aerodynamic diameter:
ca. 310 µm
Percentile:
D10
Mean:
ca. 9.3 µm
St. dev.:
0
Percentile:
D50
Mean:
ca. 950 µm
St. dev.:
0
Percentile:
D90
Mean:
ca. 1 200 µm
St. dev.:
0
Conclusions:
T-1620L was determined to have d(0.1), d(0.5) and d(0.9) values of 9.3, 350 and 1200 μm respectively, with an MMAD value of approximately 310 μm (CIPAC MT 187).

Description of key information

T-1620L was determined to have d(0.1), d(0.5) and d(0.9) values of 9.3, 350 and 1200 μm respectively, with an MMAD value of approximately 310 μm (CIPAC MT 187).

Additional information