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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
8 - 17 Feb 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes
Type of method:
method to determine freezing temperature

Test material

Constituent 1
Chemical structure
Reference substance name:
2-[[1-(chloromethyl)-2-[[4-(oxiran-2-ylmethoxymethyl)cyclohexyl]methoxy]ethoxy]methyl]oxirane
Molecular formula:
C17H29ClO5
IUPAC Name:
2-[[1-(chloromethyl)-2-[[4-(oxiran-2-ylmethoxymethyl)cyclohexyl]methoxy]ethoxy]methyl]oxirane
Constituent 2
Chemical structure
Reference substance name:
cis-1,4-bis[(2,3-epoxypropoxy)methyl]cyclohexane
Cas Number:
1197197-64-0
Molecular formula:
C14H26O4
IUPAC Name:
cis-1,4-bis[(2,3-epoxypropoxy)methyl]cyclohexane
Constituent 3
Chemical structure
Reference substance name:
trans-1,4-bis[(2,3-epoxypropoxy)methyl]cyclohexane
Cas Number:
158307-92-7
Molecular formula:
C14H26O4
IUPAC Name:
trans-1,4-bis[(2,3-epoxypropoxy)methyl]cyclohexane
impurity 1
Chemical structure
Reference substance name:
[4-(oxiran-2-ylmethoxymethyl)cyclohexyl]methanol
Molecular formula:
C11H20O3
IUPAC Name:
[4-(oxiran-2-ylmethoxymethyl)cyclohexyl]methanol
impurity 2
Chemical structure
Reference substance name:
[4-[[3-chloro-2-(oxiran-2-ylmethoxy)propoxy]methyl]cyclohexyl]methanol
Molecular formula:
C14H25ClO4
IUPAC Name:
[4-[[3-chloro-2-(oxiran-2-ylmethoxy)propoxy]methyl]cyclohexyl]methanol
impurity 3
Chemical structure
Reference substance name:
2-[[3-chloro-2-[[4-[[3-chloro-2-(oxiran-2-ylmethoxy)propoxy]methyl]cyclohexyl]methoxy]propoxy]methyl]oxirane
Molecular formula:
C20H34Cl2O6
IUPAC Name:
2-[[3-chloro-2-[[4-[[3-chloro-2-(oxiran-2-ylmethoxy)propoxy]methyl]cyclohexyl]methoxy]propoxy]methyl]oxirane
impurity 4
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: TX7E5501
- Expiration date of the lot/batch: November 10, 2018
- Purity: 87.6%
- Physical state: liquid

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Ambient temperature

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
-47.51 °C
Decomposition:
no
Remarks on result:
other: ± 0.27 °C; pressure not reported

Applicant's summary and conclusion

Conclusions:
The freezing point of -47.51 ± 0.27 °C was observed for Heloxy 107 (OECD 102).
Executive summary:

The freezing point range of Heloxy 107 was determined by placing the test material in an acetone/dry ice bath with temperature probe readings. The study was conducted in accordance with the OECD 102

method and was GLP compliant; therefore the study is considered reliable without restrictions.