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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
06, 07, 15 October 2003
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
Method Al of Commission Directive 92/69/EEC and Method 830.7200 of the
OPPTS Guidelines.
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Sponsor identification SBCAT-03
Description white powder
Lot number UK030622B
Date received 09 October 2003
Storage conditions room temperature in the dark

Data relating to the identity, purity and stability of the test material are the responsibility of the
Sponsor.

The following compositional information was supplied by the Sponsor:
The test material is a mixture of 4,4'-sulfonylbisphenol, partially salted with tetraphenyl
phosphonium ions.


Key result
Melting / freezing pt.:
>= 460.5 - <= 461.5 K
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Atm. Press. Not specified

Thermographic Data – Determination 1


 





















Thermal Event



Interpretation



Temperature



°C



K



Endotherm



Melting temperature



188.0



461



 


Thermographic Data – Determination 2


 





















Thermal Event



Interpretation



Temperature



°C



K



Endotherm



Melting temperature



188.0



461



Mean melting temperature: 461 ± 0.5 K

Conclusions:
The melting/freezing temperature of the test material has been determined to be 461 ± 0.5 K.
Executive summary:

Melting/Freezing Temperature. 461 ± 0.5 K, by differential scanning calorimetry, using ASTM E537-86, Method Al of Commission Directive 92/69/EEC and Method 830.7200 of the OPPTS Guidelines.

Description of key information

The melting/freezing temperature of the test material has been determined to be 461 ± 0.5 K.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
461 K

Additional information