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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
03 January 2006 and 31 January 2006
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2006

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Type of method:
other: Differential scanning calorimetry (DSC)

Test material

Constituent 1
Reference substance name:
LiTOFA
IUPAC Name:
LiTOFA
Details on test material:
Sponsor's identification :Reaction salt of lithium hydroxide and tall oil fatty acids (LiTOFA)
Description : off white solid
Lot number : LiTOFA_a01
Date received: 20 October 2005
Storage conditions :room temperature in the dark

Results and discussion

Melting / freezing point
Melting / freezing pt.:
> 633 K
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Atm. pressure not reported.

Any other information on results incl. tables

No defnitive signs of melting were observed during either determination at temperatures up to 633 K.

Applicant's summary and conclusion

Conclusions:
The melting point/range of the test material has been determined to be >633 +/- 0.5K.
Executive summary:

Method

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537-86, Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Results

No defnitive signs of melting were observed during either determination at temperatures up to 633 K.

Conclusion

The melting point/melting range of the test material has been determined to be >633 ± 0.5 K.