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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02/03/2018-06/04/2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Reference substance name:
Extract obtained from defatted powder of Theobroma cacao (Malvaceae) by extraction with ethanol
EC Number:
947-375-5
IUPAC Name:
Extract obtained from defatted powder of Theobroma cacao (Malvaceae) by extraction with ethanol
Test material form:
other: liquid pasty
Specific details on test material used for the study:
TEST ITEM Name C03505 CACAO EXTRAIT/PG Nr 5
Structural form Multi-constituent
CAS No N/A
EC No N/A
Reference C03505
Batch No 100507204
Purity (% w/w) PG = 76.3% w/w
Expiry date 21/11/18

Test item internal No RRCo-000138_0001
Test item description C03505 CACAO EXTRAIT/PG Nr 5
Reception date 28/11/17
Reception condition Cooled
track item TI_0007125
Received quantity (Container + content) 32,5777 g

Test item has been stored according to MSDS recommendations:
temperature - 20 °C
brightness : darkness

Results and discussion

Boiling pointopen allclose all
Key result
Boiling pt.:
132.7 °C
Atm. press.:
ca. 99 kPa
Key result
Boiling pt.:
ca. 137.7 °C
Atm. press.:
ca. 99 kPa

Any other information on results incl. tables

Initial measures were : 132°C and 137°C, a correction factor of 0,34 was used.

Mean value of te corrected measures (137,7 +132,7/2) = 135.2°C

Applicant's summary and conclusion

Conclusions:
The normal boiling point of test item was measured using the Siwoloboff method at 135.2°C +/- 3.5°C.
Executive summary:

The boiling point was performed according to the OECD 103 guideline.

The normal boiling point of test item was measured using the Siwoloboff method at 135.2°C +/- 3.5°C.