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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
thermal stability
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017-07-19 - 2017-07-20
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 113 (Screening Test for Thermal Stability and Stability in Air)
Deviations:
no
GLP compliance:
yes (incl. QA statement)

Test material

Constituent 1
Reference substance name:
Phenol, 4-amino-, reaction products with aniline, 4-methyl-1,3-benzenediamine, p-phenylenediamine, sodium sulfide (Na2S) and sulfur
EC Number:
274-987-3
EC Name:
Phenol, 4-amino-, reaction products with aniline, 4-methyl-1,3-benzenediamine, p-phenylenediamine, sodium sulfide (Na2S) and sulfur
Cas Number:
70892-38-5
Molecular formula:
not applicable
IUPAC Name:
Reaction product of 4-aminophenol, aniline, 4-​methyl-​1,​3-​benzenediamine and p-​phenylenediamine with polysulfide
Test material form:
solid: particulate/powder
Details on test material:
CAS No.: 70892-38-5
EC No.: 274-987-3
Description: dark green powder
Storage: room temperature

Results and discussion

For thermal stability study

Test substance thermally stable:
yes
Remarks:
up to 500°C
Operating temperature
Key result
Operating temp.:
> 25 - <= 500 °C
Sublimation:
no
Transformation products:
no

Any other information on results incl. tables

In the temperature range of 180 °C to 270 °C a small endothermic effect was observed. This effect cannot be assigned to melting or boiling.

Table2:    Results of the DSC-measurements

No.

Sample weight / mg

Start of effect / °C

Energy[1]/ (J/g)

Remark

PN13807

7.44

180

40 (endothermic)

Figure 3

PN13808

7.95

190

30 (endothermic)

Figure 4

No decomposition of the test item was observed up to a temperature of 500 °C.

Applicant's summary and conclusion

Conclusions:
No decomposition of the test item Leuco Sulphur Green 16 was observed up to a temperature of 500 °C.
Executive summary:

No decomposition of the test item Leuco Sulphur Green 16 was observed up to a temperature of500 °C.