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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
August 6th to 7th, 2002
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report date:
2002

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
EEC Directive 92/69
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
adopted July 27, 1995
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
Red LF 6339
IUPAC Name:
Red LF 6339

Results and discussion

Melting / freezing point
Melting / freezing pt.:
> 400 °C

Any other information on results incl. tables

After measurement, the the test item was colored dark brown and had lost about 14 % of its mass and still remained a powder. The test item did not melt under the applied test conditions.

Applicant's summary and conclusion

Conclusions:
The substance does not melt under the conditions of the test.
Executive summary:

The determination of the melting point / melting range of the test item was performed according to the EEC Directive 92/69, A.1 "Melting/Freezing temperature", December 1992 and to the OECD Guideline No. 102: " Melting point I melting range", adopted July 27, 1995.

An endothermic heat effect was observed between about 80 °C and 180 °C. An exothermic heat effect starts at about 320 °C. After the experiment, the sample still remained a powder and its colour was changed to dark brown.

In the main study (heating rate of 10 K/min from 25 °C to 400 °C) the result of the preliminary test was confirmed. The test item lost about 14 % of its mass and still remained a powder. The colour had changed from red to dark brown. Thus it is obvious that the test item did not melt under the applied conditions.

In conclusion, the test substance does not melt under the conditions of the test.