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Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2010-06-18 to 2010-06-18
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The study was conducted in accordance with EC directive 440/2008, method A.1 “Melting/Freezing Temperature”, dated 31. May 2008

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Principles of method if other than guideline:
La sustancia se calienta hasta 405 ° C en un tubo capilar de vidrio dentro de un bloque de aluminio hasta su fusión. Un segundo sistema de ensayo se establece para lograr la fusión de las sustancias con la temperatura de fusión más alta.
La sustancia se calienta en un crisol de porcelana en un horno de mufla hasta 1095 ° C de acuerdo con el protocolo de funcionamiento interno del laboratorio de ensayo (SOP 114 003 70, edición 1 de fecha 03. Septiembre de 2009).
GLP compliance:
no
Type of method:
capillary method

Test material

Constituent 1
Reference substance name:
Charcoal
EC Number:
240-383-3
EC Name:
Charcoal
Cas Number:
16291-96-6
IUPAC Name:
Carbón vegetal
Details on test material:
Name: Charcoal (Probe 2: C-Fix = 80.5%)
Batch no.: 29004
Appearance: Charcoal typic
CAS No.: 16291-96-6
EINECS-No.: 240-383-3
Purity: C-Fix = 80.5%
Expiry date: Dec. 2030
Storage: Room temperature 20 ± 5 °C, keep away from humidity

Results and discussion

Melting / freezing point
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Charcoal showed no signs of melting under the test conditions described.

Any other information on results incl. tables

The determination was performed in duplicate. In both determinations, no melting was observed up to 404°C. In an additional experiment, the test item was set into a muffle oven and heated up to 1095 °C.

No melting of the test item of charcoal (Probe 2: C-Fix = 80.5%) was detected up to a temperature of 1095°C.

Under the experimental conditions used in the study (highest temperature: 1095°C), no melting point of the test item charcoal (Probe 2: C-Fix = 80.5%) could be determined.

Applicant's summary and conclusion

Conclusions:
Since there were no signs of melting up to a temperature of >1000°C, no melting point of the test item could be determined.