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The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 20 July 2010 to 24 August 2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Compliant to GLP and testing guideline; adequate coherence between data, comments and conclusions

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
air comparison pycnometer (for solids)

Test material

Constituent 1
Reference substance name:
Copper Lead Resorcylate Salicylate Complex
EC Number:
614-455-3
Cas Number:
68411-07-4
Molecular formula:
C7H5O4-, C7H5O3- Cu , Pb
IUPAC Name:
Copper Lead Resorcylate Salicylate Complex
Details on test material:
- Name of test material (as cited in study report): LEAD-COPPER-RESORCYLATE-SALICYLATE (LC12-15)
- Substance type: multiconstituent
- Physical state: green powder
- Composition of test material, percentage of components: 11.9% of copper, 35.7% of lead, 14.1% of resorcylate and 35.7% of salicylate
- Purity test date: 20/10/2009
- Lot/batch No.: 09/201
- Expiration date of the lot/batch: 04/11/2011
- Storage condition of test material: in darkness at room temperature

Results and discussion

Density
Type:
relative density
Density:
2.726 other: no unit
Temp.:
20 °C
Remarks on result:
other: standard deviation: +/- 0.002

Any other information on results incl. tables

Assay No. 1:

Test item sample weight: 7.5150 g

Reference volume (VA): 79.330 cm3

Volume of sample cell holder: 33.071 cm3

Temperature during the assay: 20°C

 

Data

P2(PSIG)

P3(PSIG)

VP(cm3)

Mean density(g/cm3)

Mean relative density

Run No. 4

17.003

4.702

2.7475

2.7352

2.738 ± 0.002

Run No. 5

17.193

4.755

2.7434

2.7393

Run No. 6

17.063

4.719

2.7439

2.7388

Remark: The runs No. 1, 2 and 3 were not taken into account, they were not complying the quality criteria.

Assay No. 2:

Test item sample weight: 7.7003 g                  

Reference volume (VA): 79.330 cm3

Volume of sample cell holder: 33.071 cm3

Temperature during the assay: 19.8°C        

Data

P2(PSIG)

P3(PSIG)

VP(cm3)

Mean density(g/cm3)

Mean relative density

Run No. 2

17.083

4.714

2.8372

2.7140

2.713 ± 0.002

Run No. 4

17.208

4.748

2.8416

2.7098

Run No. 5

17.188

4.743

2.8370

2.7142

Remark: The runs No. 1 and 3 were not taken into account, they were not complying the quality criteria.

Applicant's summary and conclusion

Conclusions:
The relative density mean value of the test item using the gas comparison method with the stereopycnometer was D (19.9 °C / 4 °C) = 2.726 ± 0.013.