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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Boiling pt.:
101.8 °C
Atm. press.:
1 013 hPa
Decomposition:
yes
Decomp. temp.:
134
Remarks on result:
other: onset of exothermic reaction: 134 °C

Differential Scanning Calorimetry (DSC, 10 K/min)

Conclusions:
The boiling point of the substance was determined according to EU Method A.2 (Boiling Temperature). The boiling point by DSC is 101.8°C at 1013 hPa. The substance has an onset of exothermic decomposition at 134°C.
Executive summary:

The boiling point of the substance was determined according to EU Method A.2 (Boiling Temperature). The boiling point by DSC is 101.8°C at 1013 hPa. The substance has an onset of exothermic decomposition at 134°C.

Description of key information

The boiling point of the substance was determined according to EU Method A.2 (Boiling Temperature). The boiling point by DSC is 101.8°C at 1013 hPa. The substance has an onset of exothermic decomposition at 134°C.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
101.8 °C

Additional information

In accordance with REACH Regulation, Art. 3, and ECHA "Guidance for identification and naming of substances under REACH and CLP" v1.2, March 2012, substances have to be separated from solvents if this is not affecting the stability of the substance or changing its composition.

In this case, separation of water would only be possible by thermical damaging of the substance. Furthermore, it was not possible to spray dry the pigment solution as it stuck to and partly melted on the conus dryer.