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EC number: 930-890-4 | CAS number: -
Flash point
Administrative data
- Endpoint:
- flash point of flammable liquids
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 07 March - 17 September 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 017
- Report date:
- 2018
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.9 (Flash-Point)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- ISO 2719 (Determination of flash point - Pensky-Martens closed cup method)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- ASTM D93 (Standard test methods for flash point by pensky-martens closed cup tester)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- other: ASTM D7094: “Standard Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester”
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- other: UN no. ST/SG/AC.10/11/Rev.6: “Non-Viscous Flammable Liquids”
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- closed cup
- Flash point apparatus:
- other: Euraflash flash-point tester (Eralytics, Vienna, Austria)
Test material
- Reference substance name:
- (2R)-6-fluoro-2-(oxiran-2-yl)chromane
- EC Number:
- 930-890-4
- Cas Number:
- 1219915-04-4
- Molecular formula:
- C11H11FO2
- IUPAC Name:
- (2R)-6-fluoro-2-(oxiran-2-yl)chromane
- Test material form:
- liquid
- Details on test material:
- - Name of test material (as cited in study reports): JNJ-42398681-AAA (T001589)
- Physical state: liquid
- Appearence: light brown
Constituent 1
- Specific details on test material used for the study:
- - Batch n°: I16FB3011
- Analytical purity: 87%
- Expiration date: 14 March 2018
- Storage condition: at room temperature
Results and discussion
Flash point
- Key result
- Flash point:
- 133 °C
- Atm. press.:
- 1 013.25 hPa
- Remarks on result:
- other: The flash-point is automatically corrected for atmospheric pressure by the flash point tester
Any other information on results incl. tables
Preliminary test
The test cup was heated at a rate of 5± 0.5°C/minute. Starting at 25°C, an attempt was made to ignite the vapour of the test item for every 2°C temperature rise.
No flash-point was observed below the boiling temperature of the test item (i.e. 197°C). Therefore the preliminary test was repeated. The temperature of the test item at the start of the additional test was 25.0°C. Starting at 25°C the ignition source was applied for every 2°C temperature rise. A third preliminary study was carried out to confirm the result of either the first of the second preliminary test.
Main study
Three tests were performed according to the ISO Guide 2719 method. The test cup was heated at a rate of 5±0.5°C/minute. Starting at 108°C, ignition was tested for every 2°C temperature rise.
The result of the first test was > 28°C from the starting temperature of the ignition source. Two more tests were performed. In these tests, the temperature of the test item at the start of the additional test was 115°C. Starting at 115°C, ignition was tested for every 2°C temperature rise.
Applicant's summary and conclusion
- Interpretation of results:
- GHS criteria not met
- Conclusions:
- The closed cup method was applied for the determination of the flash-point of JNJ-42398681-AAA (T001589)
The flash-point of the test item was 133°C.
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