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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
Methyl (9Z,12Z,15Z)-9,12,15-octadecatrienoate
EC Number:
206-102-3
EC Name:
Methyl (9Z,12Z,15Z)-9,12,15-octadecatrienoate
Cas Number:
301-00-8
Molecular formula:
C19H32O2
IUPAC Name:
methyl octadeca-9,12,15-trienoate
Constituent 2
Chemical structure
Reference substance name:
Methyl linoleate
EC Number:
203-993-0
EC Name:
Methyl linoleate
Cas Number:
112-63-0
Molecular formula:
C19H34O2
IUPAC Name:
methyl octadeca-9,12-dienoate
Constituent 3
Chemical structure
Reference substance name:
Methyl oleate
EC Number:
203-992-5
EC Name:
Methyl oleate
Cas Number:
112-62-9
Molecular formula:
C19H36O2
IUPAC Name:
methyl (Z)-octadec-9-enoate
impurity 1
Chemical structure
Reference substance name:
Methyl palmitate
EC Number:
203-966-3
EC Name:
Methyl palmitate
Cas Number:
112-39-0
Molecular formula:
C17H34O2
IUPAC Name:
methyl palmitate
Test material form:
liquid
Specific details on test material used for the study:
Name Reaction mass of methyl linolenate
and methyl linoleate and methyl oleate
Batch no. 18010144
Appearance colourless to pale yellow liquid
Composition METHYL OLEATE [CAS 112-62-9] 17 - 23 %;
METHYL LINOLEATE [CAS 112-63-0] 12 - 20 %;
METHYL LINOLENATE [CAS 301-00-8] 47-53 %;
OTHER METHYL ESTERS 4 - 16%
CAS No. not applicable (UVCB-substance)
EINECS-No. 907-284-3
Molecular formula not available (UVCB-substance)
Molecular weight not available (UVCB-substance)
Purity GC - 50.25 % linolenate methyle
Homogeneity homogeneous
Vapour pressure unknown
Stability H2O: not stated; EtOH: not stated; acetone: not stated; CH3CN: not stated; DMSO: not stated
Solubility H2O: <0.1g/L; EtOH: >1g/L; acetone: >1g/L; CH3CN: >1g/L; DMSO: >1g/L
Production date 15. Feb. 2018
Expiry date 15. Feb. 2020
Storage Room Temperature (20 ± 5°C)

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
ca. -63.79 °C

Applicant's summary and conclusion

Executive summary:

The melting point study was performed according to the OECD Guideline 102 (Melting point / Melting Range).

The test substance has the following melting point: -63.79°C.