Registration Dossier

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

Currently viewing:

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Other quality assurance:
other: Impact Analytical standard operating procedure SOP-THR-011
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
(ethyl-3-oxobutanoato-O'1,O'3)(2-dimethylaminoethanolato)(1-methoxypropan-2-olato)aluminium(III), dimerised
EC Number:
402-370-2
EC Name:
(ethyl-3-oxobutanoato-O'1,O'3)(2-dimethylaminoethanolato)(1-methoxypropan-2-olato)aluminium(III), dimerised
Cas Number:
149057-70-5
Molecular formula:
C14H28AlNO6
IUPAC Name:
octaaluminium(3+) octakis((2Z)-4-ethoxy-4-oxobut-2-en-2-olate) octakis(1-methoxypropan-2-olate) octakis(2-(dimethylamino)ethan-1-olate)

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
ca. -38 °C

Applicant's summary and conclusion

Conclusions:
According to the DSC thermogram, no melting endotherms or crystallization exotherms were observed in the temperature range of the analysis (-90 to 50 °C). One glass transition temperature (Tg) was observed in both the first and second heating scans. The Tg was determined to be -38 °C in the second heating scan using the half height method.
Executive summary:

In an OECD 102 assay, according to the DSC thermogram no melting endotherms or crystallization exotherms were observed in the temperature range of the analysis (-90 to 50 °C). One glass transition temperature (Tg) was observed in both the first and second heating scans. The Tg was determined to be -38 °C in the second heating scan using the half height method.