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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
09 July 2018 – 12 July 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Batch n°: 2712-106
- Analytical purity: 100%
- Expiration date: not indicated
- Storage condition: at room temperature
Key result
Melting / freezing pt.:
>= -12.6 - <= 53.2 °C
Decomposition:
no
Remarks on result:
other: Multiple endotherms were observed during each test run. This is suspected to be due to the presence of different chain length components.
Remarks:
No atmospheric pressure was reported

Table 1: Table of results (screening test)

 Screening test 1st endotherm onset T (°C)  2nd endotherm onset T (°C)
 A1 -10.1  33.8
 A2 2.6   35.0
 A3  4.1  34.9

Table 2: Table of results (Test B, C, D and E)

Endotherm onset temp. (°C)

-11.4

26.0

50.5

-12.6

25.0

50.9

-11.5

25.9

50.8

-11.5

24.5

53.2

Mass of Test Item Used (mg)

8.17

11.42

9.90

8.84

Start Test Temperature (°C)

-40

-40

-40

-40

Final Test Temperature (°C)

80

80

80

80

Scan Rate (K. min-1)

1

1

1

1

Conclusions:
The melting temperature of the test item was determined to range from -12.6 to 53.5°C.

Description of key information

According to a GLP study performed according to OECD guideline 102 and EU Method A.1, the melting point range of the test substance is -12.6 to 53.2°C (K1, Dekra, 2018).

Key value for chemical safety assessment

Additional information