Tetrakis(2-ethylhexane-1,3-diolato)titanium

Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling Point)

GLP compliance:

yes

Type of method:

method according to Siwoloboff

Specific details on test material used for the study:

Test Item Name TYZOR OGT
IUPAC Name Titanium(4+)tetrakis(2-ethyl-3-hydroxyhexan-1-olate)
C.A. Name Information Not Provided by Sponsor
CAS Number 5575-43-9
Batch/Lot Number 334-300153/000012
Analysed Concentration (Provided by Sponsor) 12.92 %
Date of Manufacture September2017
Date of Expiry September2019
Appearance Pale yellow viscous liquid

Storage Condition (at JRF)
Storage Condition :
Protected from light, air and moisture.
Once opened container was kept under nitrogen blanket to prevent decomposition

Key result

Boiling pt.:

ca. 246.47 °C

Atm. press.:

ca. 760 mm Hg

TABLE1: Boiling Point/Boiling RangeValues of TYZOR OGT

Atmospheric Pressure 760 mmHg
Repli-cation	Temperature of Initiation of Bubble Formation (°C)	Temperature at which Continuous String of Bubbles were Observed (°C)	Mean Boiling Range  (°C)	Boiling Point
				(°C)	Kelvin (K)
R1	244.30	246.50	243.80 – 246.70	246.50	519.65
R2	243.80	246.20		246.20	519.35
R3	244.20	246.70		246.70	519.85
Mean				246.47	519.62
Standard Deviation				0.25	0.25
Typical Calculation
Boiling Point [in Kelvin (K)]=Observed Boiling Point(°C) + 273.15                                                          =246.50 + 273.15                                                          = 519.65

Conclusions:

The mean boiling point of TYZOR OGTwas 519.62 ± 0.25 K (246.47 ± 0.25°C) at normal atmospheric pressure (760 mm Hg) was determined by Siwoloboff method.

Executive summary:

The boiling point/boiling rangeof TYZOR OGT was determined using Siwoloboff method.

The boiling point of TYZOR OGTwas 519.65, 519.35 and 519.85 K at normal atmospheric pressure (760 mm Hg).

The mean boiling point of TYZOR OGTwas 519.62 ± 0.25 K (246.47 ± 0.25°C) at normal atmospheric pressure (760 mm Hg) [TABLE1].

The mean boiling range of TYZOR OGT was 243.80 – 246.70 °C at normal atmospheric pressure (760 mm Hg).

Description of key information

The mean boiling point of TYZOR OGT was 519.62 ± 0.25 K (246.47 ± 0.25°C) at normal atmospheric pressure (760 mm Hg) was determined by Siwoloboff method.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:

246 °C