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Diss Factsheets

Physical & Chemical properties

Density

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Endpoint:
tap density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
11-April-2017 to 13-July-2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
GLP compliance:
yes
Type of method:
pour and tap (for solids)
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: 646729
- Physical state: yellow to brownish solid
- Expiration date of the lot/batch: 19 November 2018
STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: at room temperature
Type:
pour density
Density:
0.48 g/cm³
Temp.:
23.3 °C
Remarks on result:
other: 0.48 ± 0.02 g/cm3
Key result
Type:
tap density
Density:
0.58 g/cm³
Temp.:
23.3 °C
Remarks on result:
other: 0.58 ± 0.01 g/cm3

Table 1 - Determination of Density at 23.3 °C

Replicate Empty Cylinder (g) W1 Cylinder + sample (g) W2 Sample Weight (g) W Pour Volume (mL) V Pour Density (g/mL) Tap Volume (mL) V Tap Density (g/mL)
1 65.5249 71.2808 5.7559 11.5 0.50 10.0 0.58
2 65.5291 71.2601 5.7310 12.0 0.48 9.75 0.59
3 65.5289 71.2574 5.7285 12.5 0.46 9.75 0.59
Mean         0.48   0.58
Std. Dev.         0.02   0.01
% RSD         4.4   1.2

The %RSD acceptance criterion for the triplicate determinations was met.

Conclusions:
MTDID 28640 has a pour density of 0.48 g/cm3, and a tap density of 0.58 g/cm3, both at 23.3 °C, determined according to OECD TG 109.
Executive summary:

The pour density of MTDID 28640 is 0.48 g/cm3, its tap density is 0.58 g/cm3, both at 23.3 °C. This study was conducted according to OECD TG 109 and was GLP compliant, therefore the results are considered reliable without restrictions and suitable for Risk Assessment, Classification and Labelling.

Endpoint:
density, other
Remarks:
not specified
Type of information:
not specified
Adequacy of study:
supporting study
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
documentation insufficient for assessment
Qualifier:
according to guideline
Guideline:
other: DIN 53217
Version / remarks:
Determination Of Density Of Paints, Varnishes And Similar Coating Materials - Survey Of Test Methods
Deviations:
not specified
GLP compliance:
no
Type:
density
Density:
1.12 g/cm³
Temp.:
20 °C
Conclusions:
MTDID 28640 has a density of 1.12 g/cm3 at 20°C, determined according to the DIN 53217 standard.
Executive summary:

MTDID 28640 has a density of 1.12 g/cm3 at 20°C, determined according to the DIN 53217 standard. This result was reported on the MSDS, and other than the name of the standard, no further information was provided. This standard allows for density determination via several methods such as bulk density, tap density, and the immersed body method, which is preferred. Since the specific method is unknown, the reliability of the data is not assignable.

Description of key information

MTDID 28640 has a pour density of 0.48 g/cm3, and a tap density of 0.58 g/cm3, both at 23.3 °C, determined according to OECD TG 109.

Key value for chemical safety assessment

Additional information

In the key study, the pour density of MTDID 28640 was measured to be 0.48 g/cm3, and its tap density was measured to be 0.58 g/cm3, both at 23.3 °C. This study was conducted according to OECD TG 109 and was GLP compliant, therefore the results are considered reliable without restrictions and suitable for Risk Assessment, Classification and Labelling.

A density of 1.12 g/cm3 at 20°C, was also reported on a Safety Data Sheet which cited the DIN 53217 standard. This standard allows for density determination via several methods such as bulk density, tap density, and the immersed body method, which is preferred. However the type of density determination was not reported on the Safety Data Sheet, and since the study report was not available for review, the reliability of the data is not assignable.