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Diss Factsheets

Physical & Chemical properties

Flash point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
flash point, other
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017-09-13 - 2018-01-09
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
yes
Remarks:
When the study plan was prepared the test item was identified by m- & o-terphenyl rxn mass only. Subsequently a batch number and appearance became available and these have been included in the report.
GLP compliance:
yes
Type of method:
closed cup
Flash point apparatus:
Setaflash apparatus
Specific details on test material used for the study:
Identification: Reaction mass of m-terphenyl and o-terphenyl
Appearance/Physical state: Cream colored solid
Storage conditions: Approximately 4 °C, under nitrogen in the dark
Key result
Flash point:
182 °C
Atm. press.:
100.5 kPa

Results of the flash point determination are shown in the following table:

Test Temperature (°C) Observations
21.0 No flash.
26.0
31.0
36.0
41.0
46.0
51.0
56.0
61.0
66.0
71.0 No flash. The test item was fully melted.
71.0 (fresh sample) No flash.
76.0
81.0
86.0
91.0
96.0
101.0 (fresh sample)
106.0
111.0
116.0
121.0
126.0
131.0
136.0
141.0
146.0
151.0
151.0 (fresh sample)
156.0
161.0
166.0
171.0
176.0
181.0 A blue flash spread across the sample cup.
181.0 (fresh sample) No flash.
186.0 A blue flash spread across the sample cup.
186.0 (fresh sample)
182.0 (fresh sample)
182.0 (fresh sample)
180.0 (fresh sample) No flash.
180.0 (fresh sample)
Interpretation of results:
other: EU GHS criteria not met
Conclusions:
The flash point of the test item has been determined to be 182 ± 2 °C. Atmospheric pressure: 100.5 kPa
Executive summary:

Flash Point of the test item was determined to be 182 ± 2 °C, using a closed cup equilibrium method designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

Description of key information

Flash Point of the test item was determined to be 182 ± 2 °C, using a closed cup equilibrium method designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

Key value for chemical safety assessment

Flash point at 101 325 Pa:
182 °C

Additional information

Atmospheric pressure at test-procedure was determined as 100.5 kPa. This is in slight difference to the above stated pressure for CSA, but the difference is insignificant.