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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Standard methods without GLP are reported.
Qualifier:
no guideline followed
Principles of method if other than guideline:
3 tests were applied:
- Test according to Lütolf in an open vessel. Temperature raise at 2.5 °C/min until 350 °C.
- Test in Radex (rapid detector of exothermic processes) in an open vessel. Temperature raise until 150 °C. Exposure time at 150 °C: 16 h.
- Test according to Grewer in air stream. Temperature raise at 1.2 °C/min until 350 °C.
GLP compliance:
not specified
Type of method:
other: thermal analysis
Decomposition:
yes
Decomp. temp.:
ca. 193 °C
Remarks on result:
other: The test substance undergoes an exothermic process (decomposition) starting at ca. 181 °C with a peak at 192 - 195 °C.

- Test for decomposition according to Lütolf dynamic in an open vessel. Result: First exothermic process at 190 - 350 °C. Peak: 195 °C. dTmax 28 °C.

- Test in Radex (rapid detector of exothermic processes) in an open vessel. Result: No exothermic process up to 150 °C (for 16 h).

- Test for decomposition dynamic according to Grewer in air stream. Result: First exothermic process at 181 - 209 °C. Peak at 192 °C. dTmax 56 °C.

Conclusions:
The test substance undergoes an exothermic process (decomposition) starting at ca. 181 °C with a peak at 192 - 195 °C.
Executive summary:

Three tests were performed:

- Test for decomposition according to Lütolf dynamic in an open vessel. Result: First exothermic process at 190 - 350 °C. Peak: 195 °C. dTmax 28 °C.

- Test in Radex (rapid detector of exothermic processes) in an open vessel. Result: No exothermic process up to 150 °C (for 16 h).

- Test for decomposition dynamic according to Grewer in air stream. Result: First exothermic process at 181 - 209 °C. Peak at 192 °C. dTmax 56 °C.

Description of key information

The test substance undergoes an exothermic process (decomposition) starting at ca. 181 °C.

The boiling temperature was calculated to 718 °C using the MPBPVP v1.43 tool within EpiSuite v4.1 programme.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
718 °C

Additional information