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Physical & Chemical properties

Density

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Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 2018-03-01 to 2018-04-07
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7300 (Density / Relative Density / Bulk Density)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: CIPAC Handbook Volume F, MT 3.2, “Determination of Specific Gravity or Density of Liquids or Solids”.
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method
Key result
Type:
relative density
Density:
1.185 other: dimensionless
Temp.:
20 °C

The empty pycnometer and the pycnometer with water were weighed and recorded to find out the capacity of the pycnometer. The empty pycnometer and the pycnometer with test item were weighed and recorded. The density of test item was calculated from the capacity of the pycnometer. The test was performed at 20 °C under thermostatic conditions and the obtained relative density values are found to be 1.1852 and 1.1845 for the first and second replicate, respectively. The mean relative density was found to be 1.1849 with 0.042 % of RSD.

Table 1. Determination of the capacity of the pycnometer

Replication Number

Weight of Empty Pycnometer (x) in g

Weight of Pycnometer with Water (y) in g

Water Equivalent Weight (y-x) in g

 

Volume of Pycnometer at 20 °C

V20= 1.0018 (y-x) in mL

1

20.2410

45.3819

25.1409

25.1862

2

21.0409

45.7112

24.6703

24.7147

Table 2. Determination of the relative density of the test item at 20 °C

Replication Number

Weight of Empty Pycnometer (x) in g

Weight of Pycnometer with Test Item (y’) in g

Weight of the Test Item (y’-x) in g

Density of Test Item in g/mL

(y’-x)/V20

Mean Density in g/mL

± SD

% RSD

1

20.2410

50.0927

29.8517

1.1852

1.1849

0.0005

0.042

2

21.0409

50.3165

29.2756

1.1845

Conclusions:
The relative density of the test item was found to be 1.1849 at 20.0 °C.
Executive summary:

A study was conducted according to OECD TG 109, Regulation (EC) No 440/2008 method A.3, OPPTS 830.7300 and CIPAC Handbook Volume F, MT 3.2 to determine the relative density of the test item. The density was determined in two independent determinations. Using the pycnometer method the relative density was determined to be 1.1849 at 20 °C with respect to water at 4 °C.

Description of key information

The relative density of the test item was determined to be 1.1849 at 20.0 °C.

Key value for chemical safety assessment

Relative density at 20C:
1.185

Additional information

A study was conducted according to OECD TG 109, Regulation (EC) No 440/2008 method A.3, OPPTS 830.7300 and CIPAC Handbook Volume F, MT 3.2 to determine the relative density of the test item. The density was determined in two independent determinations. Using the pycnometer method the relative density was determined to be 1.1849 at 20 °C with respect to water at 4 °C.