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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Study period:
2017-06-12 (experimental phase)
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Remarks:
in-house data with poorer documentation, but given data allows to conclude that the study was properly conducted

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
DSC measurement, glass transition / melting temperature
Deviations:
not applicable
GLP compliance:
not specified
Type of method:
differential scanning calorimetry

Test material

impurity 1
Reference substance name:
Phosphoric acid, butyl ester, branched, compd. with 2-ethyl-N-(2-ethylhexyl)-1-hexanamine
EC Number:
308-859-6
EC Name:
Phosphoric acid, butyl ester, branched, compd. with 2-ethyl-N-(2-ethylhexyl)-1-hexanamine
Cas Number:
98679-19-7
Molecular formula:
not applicable (UVCB substance)
IUPAC Name:
Phosphoric acid, butyl ester, branched, compd. with 2-ethyl-N-(2-ethylhexyl)-1-hexanamine
Test material form:
liquid

Results and discussion

Melting / freezing point
Melting / freezing pt.:
< -20 °C
Decomposition:
no

Applicant's summary and conclusion

Conclusions:
The study was performed equivalent to OECD 102 with DSC measurement on the substance to be registered itself, the test procedure is well documented and therefore reliability of Klimisch 2 has been assigned. No melting point observed above -20 °C, Glass transition was seen at -72.1 °C (onset).
Executive summary:

The study was performed equivalent to OECD 102 with DSC measurement. No melting point observed above -20 °C, Glass transition was seen at -72.1 °C (onset).