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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
other:
Version / remarks:
ASTM E 537-12 - Standard Test Method for Assessing the Thermal Stability of Chemicals by Methods of Thermal Analysis
Principles of method if other than guideline:
This test method describes the ascertainment of the presence of enthalpic changes in a test specimen, using minimum quantities of material, approximates the temperature at which these enthalpic changes occur and determines their enthalpies (heats) using differential scanning calorimetry or pressure differential scanning calorimetry.
GLP compliance:
no
Type of method:
thermal analysis
Remarks:
DSC
Key result
Remarks on result:
not determinable

DSC test in static air

No melting point detected

exothermic effect between 160 and 210 °C (∆H EXO = -50 J/g).

DSC test in static nitrogen

No melting point detected

exothermic effect between 155 and 205 °C (∆H EXO = -10 J/g).

Conclusions:
Due to the physi physical state of the substance, no melting point was detected.
DSD revealed and exothermic effect between 160 and 210 °C (∆H EXO = -50 J/g), in air and exothermic effect between 155 and 205 °C (∆H EXO = -10 J/g) in static nitrogen.


Executive summary:

The melting point was detected on the sample according to ASTM E 537-12 - Standard Test Method for Assessing the Thermal Stability of Chemicals by Methods of Thermal Analysis.

Due to the physi physical state of the substance, no melting point was detected.

DSD revealed and exothermic effect between 160 and 210 °C (∆H EXO = -50 J/g), in air and exothermic effect between 155 and 205 °C (∆H EXO = -10 J/g)  in static nitrogen.

Description of key information

No melting point detected

Key value for chemical safety assessment

Additional information

The melting point was detected on the sample according to ASTM E 537-12 - Standard Test Method for Assessing the Thermal Stability of Chemicals by Methods of Thermal Analysis.

Due to the physi physical state of the substance, no melting point was detected.

DSD revealed and exothermic effect between 160 and 210 °C (∆H EXO = -50 J/g), in air and exothermic effect between 155 and 205 °C (∆H EXO = -10 J/g)  in static nitrogen.