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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
12-03-2018 – 12-03-2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Principles of method if other than guideline:
The boiling point determination of Test item Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done as per the test guideline OECD 103.
GLP compliance:
no
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
- Name of the test material (IUPAC name): Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate- Common name: Basic Violet 4- Molecular weight: 515.7375- Molecular formula: C33H45N3O2- Smiles: CCN(CC)C1=CC=C(C=C1)C(=C2C=CC(=[N+](CC)CC)C=C2)C3=CC=C(C=C3)N(CC)CC.CC(=O)[O-]- Inchl: 1S/C31H42N3.C2H4O2/c1-7-32(8-2)28-19-13-25(14-20-28)31(26-15-21-29(22-16-26)33(9-3)10-4)27-17-23-30(24-18-27)34(11-5)12-6;1-2(3)4/h13-24H,7-12H2,1-6H3;1H3,(H,3,4)/q+1;/p-1- Substance type: Organic- Physical Appearance: greenish lustrous liquid- Stability: Stable in recommended storage conditions- Storage Conditions: Ambient Temp (23 to 27 °C)
Key result
Boiling pt.:
128.2 °C
Atm. press.:
975.9 hPa
Decomposition:
no
Remarks on result:
other: Other details not available

TEST DESCRIPTION AND RESULT

Volume of chemical used

ml/ g

1 ml

-

Nature of the Bath taken

·    Oil bath

·    Water bath

Oil bath

-

 

If oil bath is used, the type of oil

·    Liquid paraffin

·    Silicone oil

Silicone oil

-

Atmospheric pressure

hPa

975.9 hPa

 

Decomposition

Decomposition temperature (°C), if applicable

·                    Yes

·                    No

No

 

 

-

Conclusions:
The boiling point determination of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and boiling point was determine to be 128.2°C at 975.9 hPa.
Executive summary:

The boiling point determination of Test item Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point was determine to be 128.2°C at 975.9 hPa.

Description of key information

The boiling point determination of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and boiling point was determine to be 128.2°C at 975.9 hPa.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
128.2 °C

Additional information

The boiling point determination of Test item Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point was determine to be 128.2°C at 975.9 hPa.