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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
11-12-2017 – 12-12-2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Principles of method if other than guideline:
The boiling point determination of Test item 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6-methoxy-3-methylbenzothiazolium acetate (CAS No. 84051-87-6 ) was done as per the test guideline OECD 103. The method followed was according to Siwoloboff.
GLP compliance:
no
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
- Name of test material : 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6-methoxy-3-methylbenzothiazolium acetate
- Molecular formula: C19H23N4O2S.C2H3O2
- Molecular weight: 430.5264 g/mol
- SMILES: CCN(CCO)c1ccc(cc1)/N=N/c2[n+](c3ccc(cc3s2)OC)C.CC(=O)[O-]
- InChI: 1S/C19H23N4O2S.C2H4O2/c1-4-23(11-12-24)15-7-5-14(6-8-15)20-21-19-22(2)17-10-9-16(25-3)13-18(17)26-19;1-2(3)4/h5-10,13,24H,4,11-12H2,1-3H3;1H3,(H,3,4)/q+1;/p-1
- Substance type: Organic
- Physical state: Liquid
- Batch no.: YPA-2016
- Physical Appearance: free flowing blue liquid
- Stability: Stable in recommended storage conditions
- Storage Conditions: 1. Ambient Temp (23 to 27 °C) √ (Store in a cool place. Keep containers tightly closed in a dry and well ventilated place)
Key result
Boiling pt.:
108.3 °C
Atm. press.:
977.4 hPa
Decomposition:
no
Remarks on result:
other: Other details not available

Observation table & Result :

Method Details

Observations 

Remarks if, any

Guideline

OECD 103

 

 

Method

Method according to Siwoloboff

 

 

Principle of Boiling point test

The boiling point of a liquid is the temperature at which that liquid is converted to a gaseous state. It can be defined as the temperature at which the vapour pressure of the liquid becomes equal to the pressure at the surface of the liquid.

 

 

Volume of chemical used

ml/ g

1 ml

-

Nature of the Bath taken

·    Oil bath

·    Water bath

Oil bath

-

 

If oil bath is used, the type of oil

·    Liquid paraffin

·    Silicone oil

Silicon oil

-

Atmospheric pressure

hPa

977.4 hPa

-

Decomposition

Decomposition temperature (°C), if applicable

·                    Yes

·                    No

No

-

Boiling point (°C) (RESULT)

°C

108.3 °C

-

Boiling point range, if applicable

°C

-

-

Conclusions:
The boiling point determination of Test item 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6- methoxy-3 -methylbenzothiazolium acetate (CAS No. 84051 -87 -6 ) was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The mean boiling point was determine to be 108.3°C at 977.4 hPa.
Executive summary:

The boiling point determination of Test item 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6- methoxy-3 -methylbenzothiazolium acetate (CAS No. 84051 -87 -6 ) was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The mean boiling point was determine to be 108.3°C at 977.4 hPa.

Description of key information

The boiling point determination of Test item 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6- methoxy-3 -methylbenzothiazolium acetate (CAS No. 84051 -87 -6 ) was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The mean boiling point was determine to be 108.3°C at 977.4 hPa.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
108.3 °C

Additional information

The boiling point determination of Test item 2-[[4-[ethyl(2-hydroxyethyl)amino]phenyl]azo]-6- methoxy-3 -methylbenzothiazolium acetate (CAS No. 84051 -87 -6 ) was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The mean boiling point was determine to be 108.3°C at 977.4 hPa.