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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Well performed study according to accepted standard

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: company SOP
GLP compliance:
no
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
Sodium bis[3-[[1-(3-chlorophenyl)-4,5-dihydro-3-methyl-5-oxo-1H-pyrazol-4-yl]azo]-4-hydroxy-N-methylbenzene-1-sulphonamidato(2-)]chromate(1-)
EC Number:
276-067-7
EC Name:
Sodium bis[3-[[1-(3-chlorophenyl)-4,5-dihydro-3-methyl-5-oxo-1H-pyrazol-4-yl]azo]-4-hydroxy-N-methylbenzene-1-sulphonamidato(2-)]chromate(1-)
Cas Number:
71839-81-1
Molecular formula:
C34H28Cl2CrN10O8S2.Na
IUPAC Name:
Chromate(1-), bis[3-[2-[1-(3-chlorophenyl)-4,5-dihydro-3-methyl-5-(oxo-kO)-1H-pyrazol-4-yl]diazenyl-kN1]-4-(hydroxy-kO)-N-methylbenzenesulfonamidato(2-)]-, sodium (1:1)

Results and discussion

Melting / freezing point
Melting / freezing pt.:
> 278 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
278 °C
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
The substance decomposes at about 278°C and shows no melting point before.
Executive summary:

The melting point of the substance should be determined by DSC (Mettler, DSC 821e, 25 – 450°C, 3 K/min, sealed glass vial in air).

No melting but only decomposition could be observed at 278°C.