Registration Dossier

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
January 1990 - April 2015, 27 September 2014
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report Date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to
Guideline:
other: Heat stability test by ARC (Accelerating Rate Calorimeter)
Qualifier:
according to
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
no
Type of method:
other: ARC (Accelerating Rate Calorimeter)

Test material

Reference
Name:
Unnamed
Type:
Constituent
Test material form:
liquid

Results and discussion

Boiling pointopen allclose all
Key result
Boiling pt.:
386.15 K
Atm. press.:
0.21 kPa
Remarks on result:
other: MOI boiling temperature
Key result
Boiling pt.:
141.5 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: Start temperature of exothermic reaction

Any other information on results incl. tables

Result

Start temperature of exothermic reaction: 141.5°C

Discussion

Exothermic reaction of BEI would result in the polymerization of the sample compound. That start temperature of exothermic reaction is almost the same as the boiling temperature of MOI. The determination of the MOI boiling temperature would be carried out under reduced pressure.

Observed boiling point

Test 1: 113°C (0.21kPa)

Test 2: 113°C (0.21kPa)

Mean 113°C (0.21kPa)

Applicant's summary and conclusion