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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 14 to November 07, 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature

Test material

Constituent 1
Chemical structure
Reference substance name:
ethyl 2-cyclopentylidene-3-oxobutanoate
EC Number:
812-640-5
Cas Number:
95296-11-0
Molecular formula:
C11H16O3
IUPAC Name:
ethyl 2-cyclopentylidene-3-oxobutanoate
Constituent 2
Chemical structure
Reference substance name:
ethyl 2-(cyclopent-1-en-1-yl)-3-oxobutanoate
Molecular formula:
C11H16O3
IUPAC Name:
ethyl 2-(cyclopent-1-en-1-yl)-3-oxobutanoate
Specific details on test material used for the study:
Aspect : colourless to pale yellow liquid
Lot No. : SC00018589
Purity : 93.8% (sum of the three peaks)
Expiration date : June 07, 2020

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
< -50 °C
Atm. press.:
1 013 hPa
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
No freezing of the test substance was observed down to a temperature of -50.0°C (223.15 K)

Therefore: Freezing point of Ethyl Cyclopentylidene Acetoacetate
< -50.0°C (< 223.15 K).
Executive summary:

The freezing point of Ethyl Cyclopentylidene Acetoacetatewas measured according to the OECD guideline No. 102 (method of the freezing temperature).

 

No freezing of the test substance was observed down to a temperature of -50.0°C (223.15 K)

 

Therefore:

Freezing point ofEthyl Cyclopentylidene Acetoacetate< -50.0°C (< 223.15 K).