Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 613-855-5 | CAS number: 65928-65-6
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 2016
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- guideline study with acceptable restrictions
- Qualifier:
- according to guideline
- Guideline:
- other: OECD Guidelines for Testing of Chemicals, Section 1 "Physical-Chemical Properties No: 113" Screening Test for Thermal Stability and Stability in Air
- Deviations:
- no
- Qualifier:
- equivalent or similar to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Deviations:
- not applicable
- GLP compliance:
- no
- Type of method:
- thermal analysis
- Remarks:
- Differential Thermal Analysis (DTA)
- Melting / freezing pt.:
- 65 - 200 °C
- Decomposition:
- yes
- Decomp. temp.:
- 375 - 450 °C
- Remarks on result:
- other: No pressure reported
- Conclusions:
- A melting range between approx. 65 °C and 200 °C could be observed. No pressure is reported.
- Executive summary:
A differential thermoanalysis method (DTA) was used to determine the melting point which conforms to the procedure Test method A.1, "Determination of the melting point", described in the EC-Guideline.A melting range of the test item between approx. 65 and 200 °C could be observed. After the boiling process a decomposition of the substance seems to take place. This is supported by the light yellowish colour of the residue in the crucible. Between 375 °C and 450 °C another endothermic effect could be observed.
Reference
Between approx. 245 °C and 370 °C an endothermic effect was visible. This appears to be the boiling range of the test item. Additionally a decomposition of the test item seems to take place. This assumption is supported by the light yellowish colour of the residue in the crucible.
Between 375 °C and 450 °C another endothermic effect could be observed. Within this phase the decomposition of the test item seems to proceed, based on the dark-orange colour of the residue in the crucible.
Description of key information
The melting point of the substance is in the range between 65 and 200 °C and no pressure was reported.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- 127.5 °C
Additional information
"Should be considered as mean value"
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
