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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Remarks:
T
GLP compliance:
yes
Type of method:
other: capillary method

Test material

Constituent 1
Details on test material:
- Purity: > 96%

Results and discussion

Boiling point
Boiling pt.:
294.15 °C
Atm. press.:
979 hPa
Decomposition:
no

Any other information on results incl. tables

The colour of the test item did not change by the increase of temperature. The test item was bubbling from around 286°C, the boiling point of test item is 294.15°C.

Applicant's summary and conclusion

Conclusions:
The boiling point of test item is 294.15°C.
Executive summary:

The boiling point of the test substance was determined according to OECD Guideline 103. A small amount of the test item was heated in the electronic controlled sample block and the temperature around the sample was displayed. The sample was observed visually while raising the temperature. A phase transformation from liquid to vapour usually is deduced by the formation of bubbles. The test item was assessed visually for any possible changes in its appearance, consistency and colour.

According to the preliminary test boiling point was observed, therefore the samples in a glass tube were heated from 285°C to 310°C with a rate of 0.5°C/min. The colour of the test item did not change by the increase of temperature. The test item was bubbling from around 286°C, the boiling point of test item is 294.15°C.