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Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02-09-2009 / 20-10-2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Deviations:
no
GLP compliance:
yes

Test material

Constituent 1
Reference substance name:
RS-Pantolactone
IUPAC Name:
RS-Pantolactone
Constituent 2
Chemical structure
Reference substance name:
(±)-dihydro-3-hydroxy-4,4-dimethylfuran-2(3H)-one
EC Number:
201-210-7
EC Name:
(±)-dihydro-3-hydroxy-4,4-dimethylfuran-2(3H)-one
Cas Number:
79-50-5
Molecular formula:
C6H10O3
IUPAC Name:
(±)-dihydro-3-hydroxy-4,4-dimethylfuran-2(3H)-one
Details on test material:
- Name of test material (as cited in study report): RS-Pantolactone
- Physical state: Waxy Solid, white
- Analytical purity: 99.7 %
- Lot/batch No.: Bx TL 00905003
- Expiration date of the lot/batch: May 2011
- Storage condition of test material: At room temperature at about 20 °C

Results and discussion

Relative self-ignition temperature (solids)
Relative self-ignition temperature:
> 400 °C
Remarks on result:
other:
Remarks:
at atm. press. of 99.5 kPa

Any other information on results incl. tables

The determination of the relative self-ignition temperature of the test item was performed according to the Council Regulation (EC) No. 440/2008, Part A, Methods for the determination of physico-chemical properties, A.16 Relative self-ignition temperature for solids.

 

The correlation between the temperature of the oven and the sample temperature of RS-Pantolactone is shown in Figure1.

 

Using a linear increase in temperature of about 0.5 °C/min, RS-Pantolactone showed no relevant exothermic reaction. At the end of the measurement, RS-Pantolactone was completely evaporated and the cube was empty.

Applicant's summary and conclusion

Conclusions:
RS-Pantolactone is not auto-flammable, according to the criteria as described in the guideline.
Executive summary:

During this study, the self-ignition characteristics were determined. Therefore, the test item was filled into a cube and heated in an oven. The temperatures of the oven and the sample were continuously recorded while the temperature of the oven was increased to approximately 400 °C.

 

RS-Pantolactone showed no exothermic reaction. RS-Pantolactone is not auto-flammable, according to the criteria as described in the guideline.

 

The atmospheric pressure during the measurement was 99.5 kPa.