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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

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Description of key information

The particle size was determined in accordance with GLP principles and using test method OECD Guideline 110 on material as manufactured. The particle size was measured by image analysis and found to be in the range 10-105 µm.

Additional information

The particle size data provided in this report is for ADCA as manufactured. Some of the tests in this dossier have been carried out on this manufactured substance and some on micronized material. The particular grade of material used for each test is indicated below. Tests where the particle size of the tested material is unknown are also given:

Tests conducted with manufactured material (batch NF57L) are:

Appearance

HLS 2010

9F57L

Melting point

HLS 2010

9F57L

Density

HLS 2010

9F57L

Particle size

HLS 2010

9F57L

Vapour pressure

HLS 2010

9F57L

Partition coefficient

HLS 2010

9F57L

Water solubility

HLS 2010

9F57L

Surface tension

HLS 2010

9F57L

Autoflamability

HLS 2010

9F57L

Explosive properties test A14

HLS 2010

9F57L

Oxidising properties

HLS 2010

9F57L

Hydrolysis, 2010

HLS 2010

9F57L

Ready biodeg, OECD 301B

HLS 2010

9F57L

Ready bideg, OECD 301 A

HLS 2013

9F57L

Adsorption coefficient (Koc

HLS 2010

9F57L

Daphnia reproduction

HLS 2013

9F57L

ASRIT

HLS 2010

9F57L

Tests performed with commercially available micronised substance(Unifoam AZ-SO-NL), average particle size 6µm:

Acute toxicity oral

HLS 1988

100% Unifoam AZ SO-NL

Acute tox inhalation

HLS 1988

100% Unifoam AZ SO-NL

Acute tox dermal HLS

HLS 1988

100% Unifoam AZ SO-NL

Skin irritation

HLS 1988

100% Unifoam AZ SO-NL

Eye irritation

HLS 1988

100% Unifoam AZ SO-NL

Skin sensitisation

HLS 1988

100% Unifoam AZ SO-NL

Gen Tox Ames

HLS 1988

Unifoam AZ SO-L, 6µm

In vitro Chrom Abs

HLS 1989

100% Unifoam AZ SO-NL

In vivo micronucleus

HLS 1988

100% Unifoam AZ SO-NL

Tests performed with micronised material:

Explosive properties, BAM 1997, GLP/II23/270897/01

TRACEL D 205 M

3.19-27.22µm main fraction 4.10µm

Explosive properties, BAM 1995/GLP/II.23/260695/01

AZ VE-35M (Code 006035)

mean granulometery 4µm

Explosive properties, BAM 1995/GLP/II.23/260695/02

AZ VE-25M (Code 006045)

mean granulometry 5µm

Explosive properties, BAM 1995/GLP/II.23/260695/03

AZ VE-40R (Code 006064)

mean granulometry 2.2µm

Explosive properties, BAM 1995/GLP/II.23/260695/04

AZ VE-40S (Code 006065)

mean granulometry 3µm

Explosive properties, BAM 1995/GLP/II.23/260695/05

UNIFOAM AZ VE-1000 (Code 006068)

mean granulometry 7µm

Explosive properties, BAM 1995/GLP/II.23/260695/06

AZ VE-25 (Code 006225)

mean granulometry 5µm

Explosive properties, BAM 1995/GLP/II.23/260695/07

AZ VE-30R (Code 006227)

mean granulometry 3µm

Explosive properties, BAM 1997, GLP/II23/270897/02

Batch number not reported

15.7 - 50.53µm; main fraction 3.45µm

Tests perfomed for which there is no information on particle size:

Explosive properties, BAM 1998, GLP/II23/040998/01

Batch no. not reported

purity 99.8%

Ready biodegradation SafePharm OECD 301B

Batch no. not reported

20.70% carbon

Fish acute

Lot 1221 ski 3

no details of source

Daphnia acute

Lot 1221 ski 3

no details of source

Aquatic algae toxicity

2070923 F box 60

no details of source

Acute tox inhalation, Am. Ind. Hyg. Ass. J,48(2):127-132

Batch no. not reported

99.4% - source Midwest Res. Inst, Kansa, USA

Acute tox dermal MB Res. Labs

Celogen AZ 120

Source UniRoyal Chemical Co. Inc

Respiratory sensitisation J.Appl. Toxicol 9(3) 145-153

Batch no. not reported

99.4% source Midwest Res Inst. Kansas, USA

Repeat dose oral, Toxiol. and Appl,. Pharmaco.7,445-472 (1965) 2 year, rats

Batch no. not reported

no details of source

Repeat dose inhalation Fund.and Appl. Toxicology 15,308-319 90 day rat

Batch no. not reported

Source Midwest Research Institute

Repeat dose inhalation Fund.and Appl. Toxicology 15,308-319 90 day mouse

Batch no. not reported

Source Midwest Research Institute

Repeat dose inhalation, Gerlach et al, 1989. J App. Tox. 4 week guinea pig

Batch no. not reported

Source Midwest Research Institute

Gen Tox Ames

3738-4115-4117

Source Uniroyal Company Celogen AZ-130

Gen Tox Ames

205800

Source FBC Celogen AZ 120

Gen Tox Ames, J Med. 14 269-292

Batch no. not reported

no details of source

Gen Tox Ames J Med 14, 269-292

Batch no. not reported

no details of source

In vitro gene mutation

Batch no. not reported

Celogen AZ 130 source Pharmakon

In vivo micronucleus

3738, 4115, 4117

Celogen AZ 130, Pharmkon

In vivo micronucleus

Batch no. not reported

no details of source

One gen repro, Hatano Research Inst

Batch no. not reported

99.50%

Multi generation rat 2 year

Batch no. not reported

no details of source