Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

Currently viewing:

Administrative data

Link to relevant study record(s)

Referenceopen allclose all

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
weight of evidence
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
no data
GLP compliance:
not specified
Type of method:
other: no data
Melting / freezing pt.:
>= 94 - <= 102 °C
Executive summary:

The melting point of CBS is 94 - 102°C (Kirk-Othmer, 2000).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
weight of evidence
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
secondary literature
Principles of method if other than guideline:
The melting points of the products were determined by an X-4 micro-melting
point apparatus (Beijing, China).
GLP compliance:
no
Type of method:
capillary method
Melting / freezing pt.:
>= 98 - <= 100 °C
Decomposition:
no
Sublimation:
no
Executive summary:

The melting points of the N-cyclohexylbenzothiazole-2-sulphenamide was determined by an X-4 micro-melting point apparatus (Beijing, China).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
weight of evidence
Study period:
2017
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
secondary literature
Principles of method if other than guideline:
The melting points of the N-cyclohexylbenzothiazole-2-sulphenamide was determined by an X-4 micro-melting point apparatus (Beijing, China).
GLP compliance:
not specified
Type of method:
capillary method
Melting / freezing pt.:
>= 94 - <= 96 °C
Decomposition:
no
Executive summary:

The melting points of the N-cyclohexylbenzothiazole-2-sulphenamide was determined by an X-4 micro-melting point apparatus (Beijing, China).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
weight of evidence
Study period:
2017
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
method not specified
GLP compliance:
no
Melting / freezing pt.:
103 °C
Decomposition:
no
Sublimation:
no
Executive summary:

In the CRC Handbook of Chemistry and Physics 97th Edition on page 3-136 the substance N-cyclohexylbenzothiazole-2-sulphenamide is listed with a melting point of 103 °C. no further experimental details are provided.

Description of key information

The melting point of N-cyclohexylbenzothiazole-2-sulphenamide was determined in a series of experimental studies:


Kirk-Othmer, 2000: 94 - 102 °C


Tang et. al., 2019: 98 - 100 °C


Dou et. al., 2017: 94 - 96 °C


CRC Handbook of Chemistry and Physics, 97th Edition, 2017: 103 °C


 


In conclusion, the melting point is sufficiently described between 94 - 103 °C for further assessment.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
99 °C

Additional information