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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2009
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: according to valid method (DSC)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
equivalent or similar to guideline
Guideline:
other: national standard (VDI 2263)
Principles of method if other than guideline:
Differential Scanning Calorimetry (DSC)
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
3-amino-4-methoxybenzanilide
EC Number:
204-388-4
EC Name:
3-amino-4-methoxybenzanilide
Cas Number:
120-35-4
Molecular formula:
C14H14N2O2
IUPAC Name:
3-amino-4-methoxy-N-phenylbenzamide

Results and discussion

Melting / freezing point
Melting / freezing pt.:
154 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
>= 329 °C
Remarks on result:
other: The substance starts to decompose in a sealed vial at 329°C (apparatus: Mettler Toledo, DSC 821e) . The decomposition energy could not be determined precisely as the process is not complete at 450°C.

Applicant's summary and conclusion

Conclusions:
The tested melting point is 154 °C.
Executive summary:

The melting point was determined as 154°C using a Differential Scanning Calorimeter.