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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
05 August 2021 - 30 November 2021
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to other study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
>= 23.4 - <= 300.3 °C
Atm. press.:
1 013.25 hPa
Decomposition:
no

Measurement values:


Table 1: boiling point (°C and K) at 1013.25 hPa - batch 20-01 fin































































































 

1


(°C)



1


(K)



2


(°C)



2


(K)



3


(°C)



3


(K)



4


(°C)



4


(K)



5


(°C)



5


(K)



6


(°C)



6


(K)



DSC 1st spectrum


20-01 fin



23.1



296.3



81.9



355.1



176.8



450.0



255.6



498.8



289.1



562.3



300.4



573.6



DSC 2nd spectrum


20-01 fin

23.5



296.7



82.0



355.2



176.5



449.7



255.6



498.9



288.8



562.0



300.3



573.5



DSC 3rd spectrum


20-01 fin



23.5



296.7



82.1



355.3



176.6



449.8



255.6



498.8



288.9



562.1



300.2



573.4


Mean

23.4



296.5



82.0



355.2



176.6



449.8



225.6



498.8



288.9



562.1



300.3



573.5


Standard deviation

0.2



0.2



0.1



0.1



0.2



0.2



0.0



0.1



0.2



0.2



0.1



0.1



 


The boiling range of REACTION PRODUCTS OF 2,2-BIS(HYDROXYMETHYL)-1,3-PROPANEDIOL AND 3,9-DIVINYL-2,4,8,10-TETRAOXASPIRO[5.5]UNDECANE AND TRIMETHOXYMETHANE - batch 20-01 fin should be stated at (23.4 – 300.3 +/- 0.2)°C or (296.5 – 573.5 +/- 0.1K) at 1013.25 hPa.


 

Conclusions:
The determination of the boiling point was performed in accordance with Regulation (EC) No 440/2008, method A.2 “Boiling Temperature” (May 2008) and OECD Guideline No 103 “Boiling Point” (July 1995).

The boiling point of REACTION PRODUCTS OF 2,2-BIS(HYDROXYMETHYL)-1,3-PROPANEDIOL AND 3,9-DIVINYL-2,4,8,10-TETRAOXASPIRO[5.5]UNDECANE AND TRIMETHOXYMETHANE was determined by Differential Scanning Calorimetry (DSC) and should be stated as (23.4 – 300.3 +/- 0.2)°C or (296.5 – 573.5 +/- 0.1K) at 1013.25 hPa
Executive summary:

The purpose of the study was to determine the boiling point of substance REACTION PRODUCTS OF 2,2-BIS(HYDROXYMETHYL)-1,3-PROPANEDIOL AND 3,9-DIVINYL-2,4,8,10-TETRAOXASPIRO[5.5]UNDECANE AND TRIMETHOXYMETHANE


The determination of the boiling point was performed in accordance with Regulation (EC) No 440/2008, method A.2 ''Boiling Temperature'' (May 2008) and OECD Guideline No 103 “Boiling Point” (July 1995).


The boiling point of REACTION PRODUCTS OF 2,2-BIS(HYDROXYMETHYL)-1,3-PROPANEDIOL AND 3,9-DIVINYL-2,4,8,10-TETRAOXASPIRO[5.5]UNDECANE AND TRIMETHOXYMETHANE was determined by Differential Scanning Calorimetry (DSC) and should be stated as (23.4 – 300.3 +/- 0.2)°C or (296.5 – 573.5 +/- 0.1K) at 1013.25 hPa.

Description of key information

The determination of the boiling point was performed in accordance with Regulation (EC) No 440/2008, method A.2 “Boiling Temperature” (May 2008) and OECD Guideline No 103 “Boiling Point” (July 1995).


The boiling point of REACTION PRODUCTS OF 2,2-BIS(HYDROXYMETHYL)-1,3-PROPANEDIOL AND 3,9-DIVINYL-2,4,8,10-TETRAOXASPIRO[5.5]UNDECANE AND TRIMETHOXYMETHANE was determined by Differential Scanning Calorimetry (DSC) and should be stated as (23.4 – 300.3 +/- 0.2)°C or (296.5 – 573.5 +/- 0.1K) at 1013.25 hPa

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
23.4 °C

Additional information