Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 943-665-0 | CAS number: -
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- February 2016
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Deviations:
- not specified
- GLP compliance:
- not specified
- Type of method:
- differential scanning calorimetry
- Specific details on test material used for the study:
- Lot Number 3434.15
- Key result
- Melting / freezing pt.:
- > 395 - < 399 K
- Remarks on result:
- other:
- Remarks:
- DiDifferential Scanning Calorimetry
- Melting / freezing pt.:
- > 395 - < 396 K
- Remarks on result:
- other:
- Remarks:
- Capillary Method
- Conclusions:
- The RD14153 material under test was analyzed per guidelines set forth in OECD 102. A first set of determinations was carried out by Differential Scanning Calorimetry (DSC), using a TA instruments DSC2010 Calorimeter. This revealed that the material did not melt entirely homogeneous as two thermal events were uncovered at respectively 396 and 399K. A second set of determinations was carried out using an Electrothermal IA 9000 capillary melting point apparatus. This last measurement provided a melting point that coincided with a first thermal event as determined by DCS at 396K.
- Executive summary:
The RD14153 material under test was analyzed per guidelines set forth in OECD 102. A first set of determinations was carried out by Differential Scanning Calorimetry (DSC), using a TA instruments DSC2010 Calorimeter. This revealed that the material did not melt entirely homogeneous as two thermal events were uncovered at respectively 396 and 399K. A second set of determinations was carried out using an Electrothermal IA 9000 capillary melting point apparatus. This last measurement provided a melting point that coincided with a first thermal event as determined by DCS at 396K.
Reference
Melting point determinations in Kelvin:
| Determination | #1 | #2 | #3 | Average |
| DSC, mp 1 | 395 | 396 | 397 | 396 |
| DSC, mp 2 | 398 | 3** | 399 | 399 |
| Capillary | 396 | 395 | 396 | 396 |
|
|
|
|
Description of key information
Two sets of measurements were carried out for RD14153. The DSC data indicate two thermal events, one at 396K and another at 399K. The capillary measurement showed only one melting point at 396 K, which coincided with the first thermal event as determined by DSC.
Two sets of measurements were carried out for RD14156. The DSC data indicates one strong endothermal event at 396K. The capillary measurement showed a melting point at 394 K. The results are in agreement with each other in view of the estimated accuracy, and a melting point average is taken at 395K.
Melting point determinations in Kelvin for RD 14153 and RD14156.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- 396 K
Additional information
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
