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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
15-08-2013 to 23-10-2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
Guideline study performed under GLP. All relevant validity criteria were met.
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
equivalent or similar to guideline
Guideline:
other: BS4633: Method for the Determination of Crystallizing Point
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
inspected: November 2011 ; signature: March 2012
Type of method:
method to determine freezing temperature
Specific details on test material used for the study:
- Physical state: Liquid
- Storage condition of test material: Refrigerated (0 to 10°C), under nitrogen
- Other: pale yellow
Melting / freezing pt.:
< 20 °C
Atm. press.:
98.3 kPa
Remarks on result:
other: mean result of two determinations; <- 20 ± 0.5 °C or < 253 ± 0.5 K
Conclusions:
The freezing temperature of the test item has been determined to be less than 253 ± 0.5 K (or < - 20 ± 0.5 °C).
Executive summary:

The melting/freezing temperature was determined using EU Method A.1 and OECD TG 102 - crystallisation point / freezing temperature method under GLP. The mean freezing temperature of the test item has been determined to be less than 253 ± 0.5 K or less than -20 ± 0.5 °C at 1 atmosphere pressure.

Description of key information

FP: < 253 ± 0.5K (< - 20 ± 0.5°C) at 1 atm, EU Method A.1 - crystallisation point / freezing temperature method, 2013

Key value for chemical safety assessment

Additional information

Key study : EU Method A.1, 2013 : The melting/freezing temperature was determined using EU Method A.1 and OECD TG 102 - crystallisation point / freezing temperature method under GLP. The mean freezing temperature of the test item has been determined to be less than 253 ± 0.5 K or less than -20 ± 0.5 °C at 1 atmosphere pressure.