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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
3 Sept 2010 - 17 Nov 2010
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Guideline method, non-GLP

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Type of method:
thermal analysis

Test material

Constituent 1
Details on test material:
Name of test material (as cited in study report): TFEE-5
- Physical state: Colorless liquid
- Analytical purity: 97.21%
- Stability under test conditions: Test item stable
- Storage condition of test material: Ambient temperature, 10-30 °C

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
< -60 °C
Decomposition:
no
Sublimation:
no

Any other information on results incl. tables

No information is available regarding atmospheric pressure. Neither endothermic nor exothermic effects were seen in the temperature range of -60 °C to 30 °C (Figures 1, 2). Therefore, the freezing temperature of TFEE-5 is below -60 °C.

Applicant's summary and conclusion

Conclusions:
The freezing temperature of TFEE-5 is below -60 °C.
Executive summary:

The freezing temperature of TFEE-5 was measured using differential scanning calorimetry according to OECD TG103 and EC No. 440/2008.A.1. Neither endothermic nor exothermic effects were observed from -60°C to 30 °C. The freezing temperature of TFEE-5 is below -60 °C.

This study was conducted according to internationally accepted test guidelines but was not conducted according to GLP or an alternate QA standard such as ISO 17025. The study is classified as reliable with restrictions.