Reaction product of ammonium molybdate and C12-C24-diethoxylated alkylamine (1:5-1:3)

Melting point / freezing point

Administrative data

Endpoint:

melting point/freezing point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

12 May 1993

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

other: GLP compliant guideline study

Data source

Reference

Reference Type:

study report

Title:

Unnamed

Year:

1993

Report date:

1993

Materials and methods

Test guideline

Test guideline 1

Qualifier:

according to guideline

Guideline:

OECD Guideline 102 (Melting point / Melting Range)

Test guideline 2

Qualifier:

according to guideline

Guideline:

EU Method A.1 (Melting / Freezing Temperature)

GLP compliance:

yes

Type of method:

method to determine freezing temperature

Test material

Test material information

Constituent 1

Reference substance name:

Reaction product of ammonium molybdate and C12-C24-diethoxylated alkylamine (1:5-1:3)

EC Number:

412-780-3

EC Name:

Reaction product of ammonium molybdate and C12-C24-diethoxylated alkylamine (1:5-1:3)

Cas Number:

1380226-46-9

Molecular formula:

A complex mixture of species so no unique molecular formula can be given

IUPAC Name:

dimolybdenum(6+) diammonium 2-{2-[(octadec-9-en-1-yl)amino]ethoxy}ethan-1-ol heptaoxidandiide

Test material form:

liquid: viscous

Details on test material:

- Name of test material: ADDITIV 104-KONZENTRAT
- Description: Drak red liquid
- Purity: Product by process; treated as 100% pure
- Lot/batch No.: DS 147
- Expiration date of the lot/batch: March 9, 1994
- Storage condition of test material: Room temperature in the dark
- Stability under storage conditionsn and up to 60 degrees C: Stable

Results and discussion

Melting / freezing point

Key result

Melting / freezing pt.:

< -16.4 °C

Any other information on results incl. tables

Preliminary test:

During the preliminary test it was found that at 6°C, -23°C and -80°C the test substance was extremely viscous.

Main study:

A duplicate experiment was performed to determine the freezing point/freezing range of the test substance. In a duplicate experiment it was found that the test substance has no defined freezing point or freezing range. With decrease of temperature, the viscosity of the test substance increased, without showing a clear phase transition of the liquid into the solid state. At a temperature of 249.95 K (-23.2°C) in test 1 and at 256.75 K (-16.4°C) in test 2, an in the test substance Inserted stirrer could not be moved.

Applicant's summary and conclusion

Conclusions:

In conclusion, no freezing point/freezing range of the test substance could be determined. The viscosity of the test substance increases with
decreasing temperature, until finally, the test substance is completely solid.

Executive summary:

In a GLP compliant, guideline melting point/freezing point test no freezing point/freezing range of the test substance could be determined. The viscosity of the test substance increases with decreasing temperature, until finally, the test substance is completely solid.