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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental result performed using standard methods of analysis.
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Principles of method if other than guideline:
The boiling point of a liquid is the temperature at which that liquid is converted to a gaseous state. It can be defined as the temperature at which the vapour pressure of the liquid becomes equal to the pressure at the surface of the liquid.
GLP compliance:
not specified
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
Name of the test chemical: Tetraethylammonium chloride
Molecular formula:C8H20ClN
Molecular weight: 165.706 g/mol
Smiles Notation: [N+](CC)(CC)(CC)CC.[ClH-]
InChI: 1S/C8H20N.ClH/c1-5-9(6-2,7-3)8-4;/h5-8H2,1-4H3;1H/q+1;/p-1
Substance Type: Organic
Physical State: Hygroscopic white Powder
Key result
Boiling pt.:
> 300 °C
Atm. press.:
966.4 hPa
Decomposition:
no
Remarks on result:
other: Other details not available

TEST DESCRIPTION AND RESULT

Method Details

Observations

Remarks if, any

 

Guideline

OECD 103

 

The test item at 39 deg c, but no string of bubbles were observed up to 300,

inferring B.P. to be greater than 300 deg C.

Method

Method according to Siwoloboff

 

Principle of Boiling

point test

A sample is heated gradually in a tube which is immersed in a liquid bath.The sample tube is held in close contact with a thermometer and it contains a boiling capillary which is fused about1 cm above its lower end. Upon approach of the boiling temperature bubbles emerge rapidly from the lower open end of the capillary. The boiling temperature is that temperature at which, on momentary cooling, the string of bubbles stops and

liquid suddenly rises in the capillary.

 

Quantity of

chemical used

g/ml

1 g

Nature of the Bath

taken

·         Oil bath

·        

OIL

 

If oil bath is used, specify

·        

·        

SILICONE

Atmospheric

pressure

hPa

966.4

Boiling point (°C)

(RESULT)

°C

greater than 300

 

Conclusions:
The boiling point determination of Tetraethylammonium chloride is greater than 300°C at 966.4 hPa.
Executive summary:

The boiling point determination of Tetraethylammonium chloride (CAS No. 56-34-8) was done following OECD Guideline 103 and according to the method of Siwoloboff. The test item at 39 deg c, but no string of bubbles were observed up to 300, inferring B.P. to be

greater than 300 deg C and boiling point was considered to be greater than 300°C at 966.4 hPa.

Description of key information

The boiling point determination of Tetraethylammonium chloride is greater than 300°C at 966.4 hPa.

Key value for chemical safety assessment

Additional information

The boiling point determination of Tetraethylammonium chloride (CAS No. 56-34-8) was done following OECD Guideline 103 and according to the method of Siwoloboff. The test item at 39 deg c, but no string of bubbles were observed up to 300, inferring B.P. to be

greater than 300 deg C and boiling point was considered to be greater than 300°C at 966.4 hPa.