Registration Dossier
Registration Dossier
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EC number: 606-948-7 | CAS number: 2217-02-9
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- June 23, 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- comparable to guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- method according to Siwoloboff
- Key result
- Boiling pt.:
- 201.1 °C
- Atm. press.:
- 1 001 hPa
- Remarks on result:
- other: Average value ± standard deviation: 201.1 ± 0.1 ºC.
- Conclusions:
- The boiling point of D-alpha fenchol was observed at temperature of 201.1 ± 0.1°C.
- Executive summary:
The boiling point of the test substance was determined according to the OECD 103 Guideline and EU A.2 Method (Method according to Siwoloboff). The study started at a temperature gradient of 3ºC/min up to 190ºC, about 10.0˚C below the expected boiling temperature, when the heating rate was reduced to 1ºC/min. The observed value of the boiling point of D-alpha fenchol was determined to be 201.1 ± 0.1ºC under atmospheric pressure of 1001 hPa.
Reference
Table 1. The observed values of the boiling point
Sample |
Boiling temperature, °C |
The measured atmospheric pressure, hPa |
Visually |
||
1 |
201.0 |
1001 |
2 |
201.2 |
|
3 |
201.0 |
|
Average value ± standard deviation, °C |
201.1 ± 0.1 |
The three series of measurements were performed in the temperature range 100 -400ºC. Below the temperature of 190ºC, the temperature gradient of 3°C/min was used. Above 190ºC the used gradient was 1°C/min (at about 10.0°C below the expected boiling temperature).
Description of key information
Key study. Method according to OECD 103 / EU Method A.2, GLP study. The boiling point of the test item was observed at 201.1± 0.1°C.
Key value for chemical safety assessment
- Boiling point at 101 325 Pa:
- 201.1 °C
Additional information
Key study: The boiling point of the test substance was determined according to OECD 103 and EU A.2 Method (Method according to Siwoloboff). The observed value of boiling point of D-alpha fenchol was determined to be 201.1 ± 0.1ºC under atmospheric pressure of 1001 hPa.
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