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Diss Factsheets

Physical & Chemical properties

Density

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Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
March 2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
Principles of method if other than guideline:
Relative Density in accordance with EU A3 Air Comparison Pycnometer Method using Helium, SOP 060.01 Issue No. 7 issued November 2011, Expires November 2013.
Instrument: Micromeritics Accupyc 1330 TC Pycnometer LIMS 1042 (PQ Done:27/02/13, PQ Due:27/05/13)
GLP compliance:
no
Remarks:
The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Type of method:
pycnometer method
Key result
Type:
relative density
Density:
> 1.706 - < 1.713 g/cm³
Temp.:
20 °C
Remarks on result:
other: 2 tests, 5 runs per test

Test 1 (Wt. taken = 2.2547g)

Run

Volume (cm3)

Density (g/cm3)

1

1.3194

1.7089

2

1.3220

1.7056

3

1.3191

1.7093

4

1.3212

1.7065

5

1.3193

1.7090

Mean

1.3202

1.7079

Standard Deviation

0.0013

0.0017 (RSD = 0.10%)

Test 2 (Wt. taken = 2.5305g)

Run

Volume (cm3)

Density (g/cm3)

1*

1.4751

1.7155

2

1.4786

1.7115

3

1.4814

1.7081

4

1.4773

1.7129

5

1.4821

1.7074

6

1.4812

1.7084

Mean

1.4801

1.7097

 Standard Deviation  0.0021  0.0024 (RSD = 0.14%)

* Due to a run precision function of the instrument, the analysis stopped when 5 results are gained that have a variation of less than 0.05% of the cell volume, Run 1 was not used to calculate the mean value as it was ouside this acceptance criteria.

Conclusions:
Using the AccuPyc 1330TC Pycnometer, with a water bath temperature measured at 20degC +/- 0.5degC, Dechlorane plus 25 was found to have a mean relative density of 1.71 g/cm3.
Executive summary:

Experimental determination of the density of Dechlorane plus 25 was performed using an AccuPyc 1330TC Pycnometer in accordance with EU A3 Air Comparison Pycnometer Method using Helium. 2 tests of 5 runs each were performed using 2.2547 g and 2.5305 g of the sample. Test 1 resulted in a relative density of 1.7079 g/cm3 and Test 2 resulted in a relative density of 1.7097 g/cm3. Dechlorane plus 25 was found to have a mean relative density of 1.71 g/cm3.

Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
March 2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
Principles of method if other than guideline:
Relative Density in accordance with EU A3 Air Comparison Pycnometer Method using Helium, SOP 060.01 Issue No. 7 issued November 2011, Expires November 2013.
Instrument: Micromeritics Accupyc 1330 TC Pycnometer LIMS 1042 (PQ Done:27/02/13, PQ Due:27/05/13)
GLP compliance:
no
Remarks:
The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Type of method:
pycnometer method
Key result
Type:
relative density
Density:
> 1.727 - < 1.734 g/cm³
Temp.:
20 °C
Remarks on result:
other: 2 tests, 5 runs per test

Test 1 (Wt. taken = 1.7560g)

Run

Volume (cm3)

Density (g/cm3)

1

1.0139

1.7319

2

1.0150

1.7301

3

1.0154

1.7294

4

1.0162

1.7280

5

1.0163

1.7295

Mean

1.0153

1.7295

Standard Deviation

0.0010

0.0016 (RSD = 0.09%)

Test 2 (Wt. taken = 1.8613g)

Run

Volume (cm3)

Density (g/cm3)

1

1.0780

1.7267

2

1.0756

1.7304

3

1.0778

1.7269

4

1.0757

1.7303

5

1.0737

1.7336

Mean

1.0762

1.7296

 Standard Deviation  0.0018  0.0029 (RSD = 0.17%)
Conclusions:
Using the AccuPyc 1330TC Pycnometer, with a water bath temperature measured at 20degC +/- 0.5degC, Dechlorane plus 35 was found to have a mean relative density of 1.73 g/cm3.
Executive summary:

Experimental determination of the density of Dechlorane plus 35 was performed using an AccuPyc 1330TC Pycnometer in accordance with EU A3 Air Comparison Pycnometer Method using Helium. 2 tests of 5 runs each were performed using 1.7560 g and 1.8613 g of the sample. Test 1 resulted in a relative density of 1.7295 g/cm3 and Test 2 resulted in a relative density of 1.7296 g/cm3. Dechlorane plus 25 was found to have a mean relative density of 1.73 g/cm3.

Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
March 2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
Principles of method if other than guideline:
Relative Density in accordance with EU A3 Air Comparison Pycnometer Method using Helium, SOP 060.01 Issue No. 7 issued November 2011, Expires November 2013.
Instrument: Micromeritics Accupyc 1330 TC Pycnometer LIMS 1042 (PQ Done:27/02/13, PQ Due:27/05/13)
GLP compliance:
no
Remarks:
The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.
Type of method:
pycnometer method
Key result
Type:
relative density
Density:
> 1.71 - < 1.717 g/cm³
Temp.:
20 °C
Remarks on result:
other: 2 tests, 5 runs per test

Test 1 (Wt. taken = 3.7155g)

Run

Volume (cm3)

Density (g/cm3)

1

2.1716

1.7110

2

2.1702

1.7120

3

2.1696

1.7125

4

2.1698

1.7123

5

2.1730

1.7098

Mean

2.1709

1.7115

Standard Deviation

0.0014

0.0011 (RSD = 0.06%)

Test 2 (Wt. taken = 4.0436g)

Run

Volume (cm3)

Density (g/cm3)

1

2.3560

1.7163

2

2.3549

1.7171

3

2.3576

1.7152

4

2.3556

1.7166

5

2.3552

1.7169

Mean

2.3558

1.7164

 Standard Deviation  0.0011  0.0008 (RSD = 0.05%)
Conclusions:
Using the AccuPyc 1330TC Pycnometer, with a water bath temperature measured at 20degC +/- 0.5degC, Dechlorane plus 515 was found to have a mean relative density of 1.71 g/cm3.
Executive summary:

Experimental determination of the density of Dechlorane plus 515 was performed using an AccuPyc 1330TC Pycnometer in accordance with EU A3 Air Comparison Pycnometer Method using Helium. 2 tests of 5 runs each were performed using 3.7155 g and 4.0436 g of the sample. Test 1 resulted in a relative density of 1.7115 g/cm3 and Test 2 resulted in a relative density of 1.7164 g/cm3. Dechlorane plus 25 was found to have a mean relative density of 1.71 g/cm3.

Description of key information

Relative Density in accordance with EU A3, Air Comparison Pycnometer Method using Helium

Key value for chemical safety assessment

Relative density at 20C:
1.71

Additional information

The data contained in this report has been generated in a laboratory holding a current statement of GLP Compliance, issued by the UK GLP Monitoring Authority, MHRA, but not as part of a formal GLP study.