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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 21/07/2017 to 28/09/2017
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Remarks:
Test method is according to the OECD guideline 102. Test substance adequately specified. Reliability applies with restrictions, as it is not conducted under GLP conditions
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: ASTM E 537-86
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Storage condition of test material: between 15 and 35 ºC, light protected
Key result
Melting / freezing pt.:
5.8 °C
Atm. press.:
1 atm
Decomposition:
no
Remarks on result:
other: Accuracy: +/- 0.5ºC

Test 1

Weight (mg) 2.9250

Freezing point: 5.79 ºC

Test 2

Weight (mg) 2.8630

Freezing point: 5.72 ºC

Conclusions:
The freezing point of the test material was determined to be 5.8 ± 0.5 °C at atmospheric pressure
Executive summary:

The melting point of the test substance was determined according to OECD guideline 102, DSC method. Two separate measurements were performed, showing an average melting point of 5.8 ± 0.5 °C at atmospheric pressure.

Description of key information

Freezing (i.e. liquid-solid transition) occurs at 5.8 °C at atmospheric pressure (DSC, OECD 102).

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
5.8 °C

Additional information

A reliable experimental study, conducted according to OECD guideline, DSC method, is available. Despite acceptable restrictions, it is considered as a key study. The result is retained as key data.