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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
capillary method
Key result
Melting / freezing pt.:
>= 180.3 - <= 185 °C
Atm. press.:
977 hPa
Decomposition:
no
Sublimation:
no

The mean melting range ofTripiperazine dicitrate (CAS No.144-29-6) was found be180.3 °C - 185°C at 977.0 hPa.

Conclusions:
The melting point determination of Test item Tripiperazine dicitrate (CAS No. 144-29-6) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point range was found to be 180.3°C - 185°C at 977.0 hPa.
Executive summary:

The melting point determination of Test item Tripiperazine dicitrate (CAS No. 144-29-6) was done as per the test guideline OECD 102. The method followed was according toCapillary/metal block. The melting point range was found to be 180.3°C - 185°C at 977.0 hPa.

Description of key information

The melting point determination of Test item Tripiperazine dicitrate (CAS No. 144-29-6) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point range was found to be 180.3°C - 185°C at 977.0 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
180.3 °C

Additional information

The melting point determination of Test item Tripiperazine dicitrate (CAS No. 144-29-6) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point range was found to be 180.3°C - 185°C at 977.0 hPa.

Other supporting studies from authoritative handbook and MSDS also suggest that the melting point of chemical piperazine citrate was 182 -187 degree C.